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GeoAnalytical Laboratories, Inc. <br /> 2300 Maryann Dr. Turlock CA 95380 Phone(209)669-0100 Fax(209)h68-8 516 <br /> email: la b.geo@itt.net <br /> Date: 09/29/09 <br /> Report# V912316 Project: Resample Morada and Frontage Road <br /> Date Recd: 09/23/09 <br /> Jim Thorpe,Inc. <br /> PO Box 357 PO#: <br /> Lodi,CA 95241 <br /> Volatile Organic Chemistry- Quality Control <br /> GeoAnalytical Laboratories,Inc. <br /> Reporting Spike Source %REC RPD <br /> Analvte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch V002746-EPA 5030B Prepared&Analyzed:09/29/09 <br /> Blank(V002746-BLKI) <br /> 1,2-Dichloroethane ND 5.0 ug/kg <br /> Di-isopropyl E1her(DIPE) ND 10.0 <br /> Ethanol ND 400 " <br /> Ethyl tert-Butyl Ether(ETBE) ND 10.0 " <br /> Ethylene dibromide ND 10.0 <br /> Methyl tert-Butyl Ether(MTBE) 'ND 10.0 " <br /> Tert-Amyl Methyl Ether(TAME) ND 10.0 " <br /> cert-Butanol(TBA) ND 200 " <br /> Gasoline ND 1.0 mg/kg <br /> Surrogate. 1,2-Dichloroethane-d4 0.0195 0.02000 97 72-132 <br /> Surrogate:2-Bromo-/-Chloropropane 0.0169 0.01000 84 71-134 <br /> Surrogate:4-BromoJluoroben_ene 0.0202 0.02000 10/ 74-132 <br /> LCS(V002746-BSI) <br /> 1,2-Dichloroethane 64.6 5.0 ug/kg 60.00 108 80-120 <br /> Di-isopropyl Ether(DIPE) 59.3 10.0 60.00 99 80-120 <br /> Methyl tert-Butyl Ether(MTBE) 81.8 ;.10.0 60.00 136 80-120 <br /> Tert-Amyl Methyl Ether(TAME) 63.7 10.0 60.00 106 80-120 <br /> Gasoline 1.6 1.0 mg/kg 1.500 105 80-120 <br /> Surrogate:1,2-Dichloroethane-d4 0.0193 0.01000 97 72-132 <br /> Surrogate:2-Brwno-J-Chloropropane 0.0160 0.02000 80 71-134 <br /> Surrogate:4-BromoJluorobenzene 0.0202 0.02000 101 74-131 <br /> Matrix Spike(V002746-MSI) Source:V912316-01 <br /> 1.2-Dichloroethane 69:6 5.0 ug/kg 60.00 ND 116 69-140 <br /> Di-isopropyl Ether(DIPE) 59.1 10.0 60.00 ND 98 68434 <br /> Methyl tert-Butyl Ether(MTBE) 91.8 10.0 60.00 ND 153 76-179 <br /> Tert-Amyl Methyl Ether(TAME) 66.1 10.0 60.00 ND 110 69-140 <br /> Gasoline 1.3 1.0 mg/kg 1.-500 ND 88 63-143 <br /> Surrogate:1,2-Dichloroethane-d4 0.0191 0.02000 96 71-/32 <br /> Surrogate:2-Bromo-l-Chloropropane 0.0/64 0.02000 82 71-134 <br /> Surrogate:4-Bromo/luorobenzene 0.0200 0.02000 100 74-132 <br /> Certification#2585 <br />