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GeoAnalytical Laboratories, Inc. <br /> 2300 Maryann Dr. Turlock CA 95380 Phone(209)669-0100 Fax(209)668-8516 <br /> email: lab.geo@att.net <br /> Date: 08/19/09 <br /> Report# V9H0608 Project:Morada Tank Pull <br /> Date Recd: 08/06/09 <br /> Jim Thorpe,Inc. <br /> PO Bax 357 PO#: <br /> Lodi,CA 95241 <br /> CERTIFICATE OF ANALYSIS <br /> Sample ID: Waste Oil Stock Pile Date Sampled: 08/06/09 <br /> Lab ID: V9H0608-07 Time: 12:30 <br /> Sample Notes: Sampler:Steven Heune <br /> Method RL Analyte Result Units Notes Started <br /> 82608 5.0 1 sopropyl benzene(Cumene) ND ug/kg 8/10/09 10:41 am <br /> 5.0 111'p-Xylene ND ug/kg <br /> 5.0 Methyl ten-Butyl Ether.(MTBE) ND ugllkg <br /> 20,0 Methylene Chloride ND ug/kg <br /> 5.0 Monochlorobenzene ND ug/kg <br /> 5.0. n-Butylbenzene ND ug/kg <br /> 5.0 n-Propyl Benzene ND ug/kg <br /> 5.0 o-Xylene ND ug/kg <br /> 5.0 p-lsopropyltoluene ND ug/kg <br /> 5.0 see-Butyl benzene ND ug/kg <br /> 5.0 Styrene ND ug/kg <br /> 5.0 tert-Butylbenzene ND ug/kg <br /> 5:0 Tetrachloroethylene(PCE) ND ug/kg <br /> 5.0 Toluene ND ug/kg <br /> 5.0 trans-l,2-Dichloroethylene ND ug/kg <br /> 5:0 Trichloroethylene ND ug/kg <br /> 5.0 Trichlorofluoromethane ND ug/kg <br /> 5.0 Trichlorotrifluoroethane ND ug/kg <br /> 5.0 Vinyl chloride ND ug/kg <br /> Surrogate Amnt Spiked Amnt Recovered %Recovery QC Limit% Surrogate Notes <br /> 1,2-Dichloroethane-d4 20.00 20.1 100% 72-132 <br /> 2-Bromo-I-Chloropropane 26.00 21.9 110% 71-134 <br /> 4-Bromofluorobenzene .20.00 21.5 107% 74-132 <br /> M�rio b'Onoffio Richard Sereno <br /> Chemist Quality Assurance Officer <br /> Certification#2585 <br />