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Spargero Analytical Laboratory Drvision <br /> Mobile Laboratory Dmsiont&hnologyInc <br /> Scientific Division <br /> With Automotion in Mind <br /> EPA Method 8260 GCMS <br /> Matrix Spike (MS) and Matrix Duplicate Spike (MSD) <br /> Attention Mr Jeffrey Rothgery Date Sampled May 29, 1997 <br /> Apex Envirotech, Inc Date Received May 30, 1997 <br /> 7844 Madison Ave , Ste 106 Date Analyzed Jun 23, 1997 <br /> Fair Oaks, CA 95628 Invoice# 7855 <br /> Project# ERA02 009 Project Name Moore Petroleum <br /> Client ID MS/MSD (Batch) LAB ID 7984-001 MS <br /> 7984-001 MSD <br /> Matrix Water Dilution <br /> UNITS= ugh <br /> Sample Spike MS MSD QC Limits <br /> Compound Conc Added MS MSD % Rec % Rec RPD RPD % Rec <br /> 1,1-Dichloroethene ND 50 48 50 96% 100% 4% 20 61-145 <br /> Benzene ND 50 57 59 114% 118% 3% 20 76-127 <br /> Trichloroethene ND 50 51 52 102% 104% 2% 20 71-135 <br /> Toluene ND 50 54 55 108% 110% 2% 20 76-130 <br /> Chlorobenzene ND 50 49 50 98% 100% 2% 20 75-130 <br /> ppb=parts per billion=ugR=micrograms per liter <br /> ppm=parts per million=uglml=micrograms per milliliter <br /> ND=Not Delected Compound(s)may be present at concentrabons below the detection limit <br /> Jul 3, 1997 <br /> R L .lames, Principal Chemist Date Reported <br /> SPARGER TECHNOLOGY ANALYTICAL LABORATORY INC IS CERTIFIED BY THE STATE OF CALIFORNIA <br /> DEPARTMENT OF HEALTH SERVICES AS A HAZARDOUS WASTE TESTING LABORATORY <br /> 0 {Carl cation No 1614) <br /> 8260msw <br /> 3050 Fite Circle Suite 112 o Sacramento Colifornio 95827 0 (996) 362-8947 • FAX(946) 362-0947 <br />