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' I 10 Second Avenue South,#137,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> hap//www mccamnbell.com E-mail main@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID Shaugncssy Estate Date Sampled 10/09/98 <br /> 4005 North Wilson Way Date Received 10/15/98 <br /> Stockton,CA 95205 Client Contact Tun Cuellar Date Extracted 10/16/98 <br /> Client P O Date Analyzed 10/16/98 <br />' Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 97044 97045 97046 <br /> Reporting Limit <br />' Client ID MW8-40 MW9-30 MW940 <br /> Matrix S S S S W <br />' Compound Concentration* ug/kg ug/L <br />' Di-isopropyl Ether(DIPS) ND ND ND 50 1 0 <br /> Ethyl tert-Butyl Ether(ETBE) ND ND ND 50 10 <br />' Methyl-tert Butyl Ether(MTBE) 5 3 ND ND so 1 0 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND 50 1 0 <br /> tert-Butanol ND ND ND 25 50 <br /> Surrogate Recoveries(%) <br />' Dibromoiluoromethane 107 104 105 <br />' Comments <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> 1 <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br /> 1 <br />