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460 <br /> 1]0 Second Avenue South,#D7, Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax :925-798-1622 <br /> 24 http://www.mccampbell.com E-mail: main@mccampbell.com <br /> mccampbell.com <br /> ary <br /> J <br /> Advanced GeoEnvironmental <br /> Client Project ID: #96-0229;Pacific Car Date Sampled: 05/14/98 <br /> L <br /> 4045 North Wilson Way Wash <br /> Date Received: 05/15/98 <br /> E <br /> Stockton,CA 45205 Client Contact: Tim Cuellar I Date Extracted: 05117-05118198 <br /> Client P.O: Date Analyzed: 05/17-05/18/98 <br /> Volatile Organics By GCWS <br /> r.. EPA method 8260 <br /> Lab ID 89341 <br /> Client ID MW-615-14-98 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone' ' ND<150 Ethylbenzene 2600 <br /> 4 Benzene 5400 Hexachlorobutadiene ND<85 <br /> Bromobenzene ND<85 lodomet}tane ND<85 <br /> Bromochlaromethane ND<85 Isopropylbenzene ND<85 <br /> Bromodichloromethane ND<85 p-isopropyl toluene ND<85 <br /> •.. Bromoform ND<85 Methyl butyl ketone' ' ND<85 <br /> Bromomethane ND<85 Methylene Chloride"' ND<85 <br /> n-Butyl benzene ND<85 Methyl ethyl ketone'` ND<85 <br /> sec-Butyl benzene ND<85 Methyl isobuty!ketoneND<85 <br /> Cert-Butyl benzene 230 Methyl Cert-Butyl Ether(MTBE) --- <br /> Carbon Disulfide ND<85 Naphthalene 1100 <br /> Carbon Tetrachloride ND<85 n-Propyl benzene 440 <br /> Chlorobenzene ND<85 Styrene' ND<85 <br /> Chloroethane ND<85 1,1,1,2-Tetrachloroethane ND<85 <br /> 2-Chloroethyl Vinyl Ether"' ND<85 1,1.2,2-Tetrachloroethane ND<85 <br /> Chloroform ND<85 Tetrachloroethene ND<85 <br /> Chloromethane ND<85 Toluene"' 101000 <br /> 2-Chlorotoluene ND<85 1.2.3-Trichlorobenzene ND<85 <br /> 4-Chlorotoluene ND<85 1.2.4-Trichlorobenzene ND<85 <br /> Dibromochloromethane ND<85 1.1.1-Trichloroethane ND<85 <br /> 1,2-Dibromo-3-chloropropane ND<85 1.1?-Trichloroethane ND<85 <br /> +r.r Dibromomethane ND<85 Trichloroethene ND<85 <br /> 1,2-Dichlorobenzene ND<85 Trichlorotluoromethane ND<85 <br /> 1.3-Dichloroben2ene ND<85 1,2.3-Tiichloropropane ND<85 <br /> 1.4-Dichlorobenzene ND<85 1,.2.4-Trimethyl benzene 2000 <br /> Dichlorodifluoromethane ND<85 1.3,5-Trimethylbenzene 440 <br /> 1.1-Dichloroethane ND<85 Vinyl Acetate""' ND<85 <br /> 1.2-Dichloroethane N13<85 Vinyl Chloride'." ND<85 <br /> 1,1-Dichloroethene ND<85 Xylenes,total '°' 14,000 <br /> cis-1.2-Dichloroethene ND<85 <br /> trans-1,2-Dichloroethene ND<85 <br /> 1,2-Dichloropropane ND<85 <br /> 1.3-Dichloropropane ND<85 <br /> 2.2-Dichloropropane ND<85 Comments: <br /> 1,1-Dichloropropene ND<85 Surrogate Recoveries('%o) <br /> cis-1,3-Dichloropropene ND<85 Dibromotluoromethane 100 <br /> 1� trans-1,3-Dichloropropene ND<85 Toluenc-d8 94 <br /> Ethylene dibromide ND<85 4-Bromotluorobenzene 88 <br /> water and vapor samples are reported in ug1L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L. <br /> Reporting limits unless otherwise stated: water samples 1.0 ug/L-, vapor samples 0.5 ug/L; solid and sludge samples 5 ug/kg; wipes <br /> i' 0.2ug/wipe ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (1) 2-butanone; (g) 4-methyl-2 <br /> arm pentanone or isopropylacetone; (h) lighter than water immiscible sheen is present; (i)liquid sample that contains greater than --5 vol. % <br /> sediment,0)sample diluted due to high organic content;(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte;(1)methylbenzene;(m)acetic acid ethenyl ester;(n)chloroethene;(o)dimet (benzenes. <br /> DHS Certification No. 1644 // Edward Hamilton,Lab Director <br />