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' CAST <br /> . LE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive,Atwater,CA 95301 Phone (209)384-2930 <br /> Certificate#2480 Fax (209)384-1507 <br /> Advanced GeoEnvironmental, Inc Client Protect ID Pac Car Wash Method EPA 503018015M,8020 <br /> of Northern California Reference Number 6371 (1-20) Instrument ID Var-GC1 <br /> 837 Shaw Road Sample Description Water Extracted 12-05-03 <br /> Stockton, CA 95215 Analyst Jim Phillips Analyzed 12-05-03 <br />' Attn Tim Cuellar Reported 12-18-03 <br />' QUALITY CONTROL DATA REPORT <br />' ANALYTE Gasoline MTBE Benzene Toluene Ethyl Benzene Total Xylenes <br />' Spike Concentration 110 1 56 094 7 19 1 84 922 <br /> Units uglL ug/L ug/L ug/L ug/L ug/L <br /> LCS Batch# VW-D053 VW-D053 VW-DO53 VW-D053 VW-DO53 VW-D053 <br /> LCS %Recovery 967% 999% 980% 986% 105% 103% <br /> Surrogate Recovery 103% 1111% 101% 101% 101% 101% <br />' Control Limits 70-130% 70-130% 70-130% 70-130% 70-130% 70-1-30% <br />' MS/MSD Batch# VW-DO53 VW D053 VW-D053 VW-D053 VW-DO53 VW-DO53 <br /> Spike Concentration 110 1 56 0 938 719 1 84 922 <br />' MS % Recovery 899% 669% 861% 959% 102% 101% <br /> Surrogate Recovery 103% 104% 104% 104% 104% 104% <br /> MSD% Recovery 91 3% 728% 869% 957% 100% 101% <br /> Surrogate Recovery 100% 999% 999% 999% 999% 999% <br /> Relative% Difference 144% 765% 0900% 0299% 1 45% 0 112% <br />' Methanol Blank ND ND ND ND ND ND <br /> Surrogate Recovery 946% 954% 954% 954% 954% 954% <br /> The LCS(Laboratory Check Sample)is a control sample of known, interferent free matrix that is fortified with representative analytes and <br /> analyzed using the same reagents, preparation and analytical methods employed for the samples The LCS %recovery is used for validation <br /> of sample batch results Due to matrix effects,the OC limits and recoveries for MS/MSD's are advisory only and are not used to accept or <br /> reject batch results <br /> I <br /> ANALYST APPROVED BY ' <br /> Cla Cone Jamesq Phillips <br /> /laboratory Director <br /> I <br />