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110 2nd Avenue South #D7—Pacheco CA 94553 5560 <br /> McCampbel! Analytical Inc Telephone 925-798-1620 Fax 92$-798-1622 <br /> + Mr)l/www sn=rnpbell com E mad mam @mccampbell com <br /> C SUMMARY REPORT FOR SW8260B <br /> Matrix S WorkOrder 0210042 <br /> IEPA Method SW8260B Extraction SW5030B BatchlD 4233 Spiked Sample ID 0210042-003A <br /> ampound Sample Spiked MS* MSD* MS-MSD' LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> G <br /> dig/Kg pg/Kg %Rec %Rec i % RPD %Rec %Rec %RPD Low High <br /> tent-Amyl methyl ether(TAME) ND 50 868 868 00941 924 926 0 151 70 130 <br /> Methyl-t-butyl ether(MTBE) ND 50 81 9 808 1 32 859 873 161 70 130 <br /> Dusopropyl ether(RIPE) ND 50 101 102 0 319 102 106 327 70 130 <br /> Ethyl tert-butyl ether(EI BE) ND 50 91 8 91 5 0 319 95 6 966 0 970 70 —130 <br /> %S51 <br /> 950 100 942 925 1 90 102 103 1 33 70 130 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions <br /> NONE <br /> lie <br /> MS=Matrix Spike MSD=Matrix Spike Duplicate LCS=Laboratory Control Sample,LCSD=Laboratory Control Sample Duplicate RPD=Relative Percent <br /> Deviation <br /> N/A=not enough sample to perform matrix spike and matrw spike duplicate <br /> N R=analyte concentration m sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or <br /> analyte content <br /> %Recovery=100'(MS-Sample)/(Amount Spiked) RPD=100'(MS–MSD)I(MS}MSD)'2 <br /> MS and I or MSD spike recoveries may not be near 100° or the RPDs near 0%,if a)the sample is inhomogenous AND contains significant concentrations of <br /> Ianalyte relative to the amount spiked or b)if that specific sample matrix interferes with spike recovery <br />