Laserfiche WebLink
' CASTLE ANALYTICAL LABORATORY <br /> • Environmental Testing Services 2333 Shuttle Drive Atwater,CA 95301 Phone (209)384-2930 <br />' Fax (209)384-1507 <br /> Advanced Geo Environmental, Inc Client Project ID Pacific Car Wash Method EPA 5030/8260 <br />' of Northern California Reference Number 5947 Instrument ID HP Series 11 <br /> 837 Shaw Road Matrix Sod Prepared 08-01-03 <br /> Stockton CA 95215 Analyst S Foster Analyzed 08-01-03 <br /> Attn Tim Cuellar Reported 08-11-03 <br /> 1 <br /> QUALITY CONTROL DATA REPORT <br />' SPIKE ID VSMS-8013 <br /> Reporting BLANK Spiking Control %R <br />' <br /> Limit Result Level Spike Limits <br /> mg/K. m /K mg/K_ %R <br /> COMPOUNDS <br /> t-But I Alcohol(t-BA) 080 ND 300 760% 70-130 <br /> Methyl t-but I ether MTBE) 0 010 ND 0 100 700% 70-130 <br /> Diiso ro 1 ether(DIPE) 0 010 ND 0 100 708% 70-130 <br /> Ethyl t-But f ether(ETBE) 0 010 ND 0 100 872% 70-130 <br /> t-Am I methyl ether(TAME) 0 010 ND 0 100 840% 70-130 <br /> 1 2-Dlchloroethane(1 2-DCA) 0 010 ND 0 100 119% 70-130 <br /> Ethylene dlbromide(EDB) 0 010 ND 0 100 864% 70-130 <br /> Surrogates <br /> 1 2-Dichloroethane-d4 0 010 113% 0 400 107% 70-130 <br />� . Toluene-d8 0 010 999% 0 400 101% 70-130 <br /> Spiking MATRIX MATRIX %R %RPD <br /> Level SPIKE SPIKE DUP Limits <br /> m /Kg %R %R <br /> COMPOUNDS <br /> t-Hut I Alcohol(t-BA) 300 644% 603% 70-130 656% <br /> Methyl t-but I ether (MTBE) 0 100 126% 112% 70-130 118% <br /> Dusopro I ether(DIPE) 0 100 100% 952% 70-130 532% <br /> Ethyl t-But I ether(ETBE) 0 100 126% 114% 70-130 107% <br /> t-Ami methyl ether TAME 0 100 104% 940% 70-130 898% <br /> 1 2-Dichloroethane(1,2-DCA) 0 100 972% 796% 70-130 199% <br /> Ethylene dibromlde(EDS) 0 100 948% 680% 70-130 329% <br /> Surrogate <br /> 1,2-Dichlaroethane-d4 0 400 978% 123% 70-130 227% <br /> Toluene-d8 0 400 910% 133% 70-130 377% <br /> I <br /> The LCS(Laboratory Check Sample)Is a control sample of known, Interferent free matrix that is fortified with representative analytes and <br /> analyzed using the same reagents preparation and analytical methods employed for the samples The LCS%recovery Is used for validation <br /> of sample batch results Due to matrix effects,the QC limits and recoveries for MSIMSD's are advisory only and are not used to accept or <br /> reject batch results <br /> f <br /> f <br />' ANALYST APPROVED BY <br /> 0/- <br /> Cilia/ 6Ja es Phillips <br /> Iboratory Director <br />