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December 15, 2004 Lab ID STK438223 Customer 3014626 Micheline Doyle Kipf Quality Control. Organic QC 3520C 11/29/2004 A225 All preparation quality controls are within established criteria, except The following note applies to bts(2-Ethylhexyl)phthalate 210 The method blank was positive However, samples reported were either ten times greater than the blank concentration or non detect and accepted The following note applies to 2,4-Dtchlorophenol, bis(2-Chloroethoxy)methane, 2-Chlorophenol, 2-Nttrophenol 305 LCS not within Acceptance Range (AR) Data could not be confirmed by reanalysis Results were reported with client approval The following note applies to Dtbenzo(a,h)anthracene, Benzo(b)fluoranthene, Benzo(k)fluoranthene, Dimethylphthalate, Di-n-octylphthalate 310 LCS above Acceptance Range (AR) Samples which were non detect for this analyte were accepted The following note applies to Acenaphthylene, 1,2-Diphenylhydraztne, Butylbenzylphthalate, N-Nitrosodtphenylanune, Pyrene 320 LCS not within Acceptance Range (AR) Data was accepted based on the BS/BSD recovery The following note applies to 2,4,6-Trichlorophenol, 2,4-Dichlorophenol, 2-Chlorophenol, 2-Nttrophenol, 3,3'-Dtchlorobenztdine, Hexachlorobenzene, Phenol 410 Relative Percent Difference (RPD) not within Maximum Allowable Value (MAV) Data was accepted based on the LCS or CCV recovery The following note applies to 2,4,6-Trichlorophenol, 2,4-Dtchlorophenol, bis(2-Chloroethoxy)methane, 2-Chlorophenol, 2-Nttrophenol, 3,3'-Dichlorobenztdtne, Pentachlorophenol, Dtethylphthalate, Dtmethylphthalate 435 Sample matrix may be affecting this analyte Data was accepted based on the LCS or CCV recovery 5030B 11/30/2004 A233 All preparation quality controls are within established criteria 625 12/08/2004 A - GM201 All analysts quality controls are within established criteria, except The following note applies to 3,3'-Dtchlorobenztdtne, Benzidine, Chrysene, Pyrene 360 CCV above Acceptance Range (AR) Samples which were non detect for this analyte were accepted 826013 11/30/2004 A - GM207 All analysts quality controls are within established criteria, except The following note applies to tert-Butanol 355 CCV not within Acceptance Range (AR) Results were reported with client approval Case narrative continued on next page STK438223 Case Narrative Page 2