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' CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive, Atwater, CA 95301 Phone (209) 384 2930 <br />' Certificate #2079 Fax (209) 384 1507 <br /> Advanced GeoEnvironmental, Inc Client Project ID Cal Fuels Method EPA 503018015M 8020 <br />' of Northern California Reference Number 1532 Instrument ID Var-GC1 <br /> 4005 North Wilson Way Matrix Water Prepared 4-13-98 <br /> Stockton CA 95205 Analyst Jim Phillips Analyzed- 4-1398 <br /> Alin Tim Cuellar Reported 4 22 98 <br />' QUALITY CONTROL DATA REPORT <br />' ANALYTE Gasoline MTBE Benzene Toluene Ethyl Benzene Total Xylenes <br /> Spike Concentration 100 1 00 1 00 1 00 1 00 200 <br /> Units ug/L ug/L ug/L ug/L ug/L ug/L <br />' LCS Batch # VG-4138W VB-4128W VB-4138W VB-4138W VB 4138W VB 4138W <br /> LCS % Recovery 94 7% 107% 92 1% 990% 97 6% 99 2% <br /> Surrogate Recovery 101% 98 5% 98 5% 98 5% 98 5% 98 5% <br /> Control Limits 70 130 % 70 130 % 70130 % 70 130 % 70-130 % 70-130 % <br />' NISIMSD Batch # VG-4138W VI3 4138W V13-4138W VB-4138W VB-4138W VB 4136W <br /> MS % Recovery 84 1% 76 8% 78 8% 870% 85 2% 84 3% <br /> Surrogate Recovery 89 3% 88 9% 889% 88 9% 889% 88 9% <br /> tMSD % Recovery 89 7% 82 8% 845% 806% 846% 847% <br /> Surrogate Recovery 91 2% 87 7% 87 7% 87 7% 87 7% 87 7% <br />' Relative % Difference 5 89% 5 53% 6 52% 6 75% 0676% 0424% <br /> Methanol Blank NO NO NO ND ND NO <br />' Surrogate Recovery 104% 104% 104% 104% 104% 104% <br /> The LCS {Laboratory Check Sample► is a control sample of known, interferent free matrix that is fortified with representative analytes and <br /> analyzed using the same reagents, preparation and analytical methods employed for the samples The LCS % recovery is used for validation <br />' of sample batch results Due to matrix effects, the QC limits and recoveries for MSIMSD's are advisory only and are not used to accept or <br /> reject batch results <br /> J <br />' ANALYST L C APPROVED BY .(�?IA <br /> C rr J Cone / Jams C P rllrps <br /> E rronmental Lab Director <br />