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CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services P 0 Box 1360 Winton, CA 95388 Phone {209) 384-2930 <br /> Certificate #2079 Fax 12091 384-1507 <br /> Advanced GeoEnvironmental, Inc Client Project ID Cal Fuels Sampled See Below <br /> of Northern California Reference Number 975 Received 12-24-96 <br /> 1803 West March Lane, Suite A Sample Description Water Extracted 12-31-96 <br /> Stockton, CA 95207 Sample Prep/Analysis Method 8015M, 8020 Analyzed 12-31-96 <br /> Attn Tim Cuellar Lab Numbers 975-12W, 13W, 14W, 15W Reported 1-7-97 <br /> TOTAL PETROLEUM HYDROCARBONS - GASOLINE RANGE <br /> WITH BTEX DISTINCTION <br /> ANALYTE REPORTING LIMIT SAMPLE ID SAMPLE ID SAMPLE 1D SAMPLE ID <br /> B3 H2O 84-H20 66-112O 87-1-12O <br /> fug/L] fug/L1 fug/L1 lug/Ll (ug/L) <br /> MTBE 050 ND ND ND ND <br /> BENZENE 050 16000 710 8600 46 <br /> TOLUENE 0 50 28000 ND 370 ND <br /> ETHYL BENZENE 0 50 3000 29 530 ND <br />• TOTAL XYLENES 060 15000 24 680 ND <br /> GASOLINE RANGE <br /> HYDROCARBONS 50 140000 2300 27000 820 <br /> Report Limit Multiplication Factor 1000 20 200 10 <br /> Date Sampled 12 19-96 12-19-96 12-20-96 12-2096 <br /> Surrogate % Recovery FID 104%!Pio 103% FID 110%1 PID 506% FID 1G4%1 PID 100% FID 1 f0%!Pro 106% <br /> '-F—..ncnt ID ` AR-GC1 VAR-GC1 VAR-GC i VAR-GC'k <br /> Practical Quantitation Limit = Reporting Limit x Report Limit Multiplication Factor <br /> Analytes reported as ND were not detected or below the Practical Quantitation Limit <br /> ANALYST APPROVED BY <br />• Clan J Cone Ja es Phillips <br /> nvironmental Lab Director <br />