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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAWBELL ANALYTICAL INC Telephone 925-798-I620 Fax 925-798-1622 <br />' http//www mccampbell corn E-mail main@mccampbell corn AJ <br /> Advanced GeoEnvironmental Client Project ID Cal Fuels Date Sampled 10/19/99 <br /> 4005 North Wilson Way Date Received 10/21/99 <br />' Stockton, CA 95205 Client Contact Tun Cuellar Date Extracted 10/23-I0/26/99 <br />' Client P O Date Analyzed 10/23-10/26/99 <br /> Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br />' Lab ID 23823 23824 23825 <br /> Reporting LimitClient ID VW 1 AW 1B AW 2B <br />' Matrix W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPS) ND<63 ND<17 ND<8 5 5 0 1 0 <br />' Ethyl tent-Butyl Ether(ETRE) ND<63 ND<17 ND<8 5 50 1 0 <br /> lie Methyl-tert Butyl Ether(MTBE) 85 ND<17 ND<8 5 .50 1 0 <br /> tert-Amyl Methyl Ether(TAME) ND<63 ND<17 ND<8 5 50 1 0 <br /> tert-Butanol 83 25 1 1 25 50 <br /> Surrogate Re,overies(%) <br /> Dibromofluoromethane 103 100 100 <br /> Comments <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC 1 SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol ON.sediment, 0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br /> f <br /> E <br />