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110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> r McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> t //www mrmmpbell corn E-mail main@mccampbell com <br /> Date Sampled 07/16-07/17/98 <br /> Advanced GeoEnvironmental Client Project ID Cal Fuels <br /> 4005 North Wilson Way <br /> Date Received 07/22/98 <br /> Stockton,CA 95205 Client Contact Tim Cuellar Date Extracted 07/29/98 <br />! Client P O Date Analyzed 07/29-07/30/98 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab 1D 92556 <br /> Client 1D MW 11-7/17198 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone` 29 Elhylbenzene ND <br /> Benzene ND Hexachlorobutadiene ND <br /> Bromobenzene ND lodomethane ND <br /> C Bromochloromethane ND lsopropylbenzene ND <br /> Bromodichloromethane ND p-Isopropylloluene ND <br /> Bromoform ND Methyl butyl ketone' ' ND <br /> Bromomethane ND Methylene C blonde"' ND <br /> n Butyl benzene ND Meth)I ethyl ketone" 69 <br /> sec-Butyl benzene ND Methyl isobulvl ketone' ND <br /> tert-Butyl benzene ND Methvl ten-Birt}l Ether(MTBE) --- <br /> Carbon Disulfide ND Napthalene ND <br /> Carbon Tetrachloride ND n-Propyl benzene ND <br /> Chlorobenzene ND Styrene, ' ND <br /> Chloroelhane ND 1 1 1 2 Tetrachloroethane ND <br /> 2 Chloroethyl Vinyl Ether" ND 1 1 2 2-Tetrachloroethane ND <br /> Chloroform ND Tetrachioroethene 16 <br /> Chloromethane 3l Toluene" ND <br /> 2-Chlorotoluene ND 1 2 3 Trichlorobenzene ND <br />! 4-Chlorotoluene ND 1 2 4 Ti chlorobenzene ND <br /> Dibromochlommethane ND 1 1 1 Tiichloioethane ND <br /> 1 2-Dibromo 3-chloropropane ND 1 1 2-Trichloroethane ND <br /> Dibromomethane ND Trichloroethene ND <br /> l2-Dichlorobenzene ND Tnchlorolluoromethane ND <br /> I 3-Dichlorobenzene ND 1 2 3-Tnchloropropane ND <br /> 14-Dichlorobenzene ND 1 2 4-Trimeth)ibenzene ND <br /> Dichlorodifluoromethane ND 1 3 5-Trimethylbenzene ND <br /> 1 1-Dichloroethane ND Vmyl Acetate""' ND <br /> 1 2-Dichloroethane ND Vim I C hloi ide"" ND <br /> 1 1-Dichloroethene ND Xylencs,total `0} ND <br /> cis-1,2-Dichloroethene ND <br /> trans-1 2-Dichloroethene ND <br /> 1 2-Dichloropropane ND <br /> 1 3-Dichloropropane ND <br /> 2 2-Dichloropropane ND Comments <br /> I 1-Dichloropropene ND Su rrogate RecoN cries(%) <br /> cis-1 3-Dichloropropene ND Dibromo 11 Uoro methane 111 <br /> trans-l3-Dichloropropene ND Toluene-d8 99 <br /> Eth}lene-di bra m1de ND 4-Bromotluorobenzene 131 <br /> i ,+ater and vapor samples are reported in ug/L,soil and sludge samples in ug/l.g,a ipes in ug/µipe and all TCLP/SPLP extracts in ug/L <br />` Reporting limits unless otherwise stated water samples 1 0 uglL, %apor samples 05 ug/L solid and sludge samples 5 ug/kg wipes <br /> 0 2ug/tripe ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone, (e) dichloromethane (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present (i)liquid sample that contains greater than —5 vol % <br /> sediment,0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte (1)methylbenzene,(m)acetic acid ethenyl ester (n)chhiroetherie (o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />