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1 <br /> 110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> F4McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> I http I/%%ww mccamnbellsom E-mail main@mccampbell cam <br /> IAdvanced GeoEnvirorimental Client Project ID Cal Fuels Date Sampled 07116-07/17198 <br /> 40Q5 North Wilson Way Date Received 07/22/98 <br /> I <br /> Stockton, CA 95205 Client Contact Tim Cuellar Date Extracted 07/29/98 <br /> Client P O Date Analyzed 07/29-07/30/98 <br /> Volatile Organics By GUMS <br /> EPA method 8260 <br /> I Lab ID 92558 <br /> Client ID AW-IB/7/17/98 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone" ND<400 Ethylbenzene 810 <br /> Benzene 3900 Hexachlorobutadiene ND<100 <br /> Bromobenzene NEK100 lodomethane ND<100 <br /> I Bromochloromethane ND<100 Isopropylbenzene ND<100 <br /> Bromodichloromethane ND<100 p-Isopropyl toluene ND<100 <br /> Bromoform ND<100 Methyl butyl ketone' ' ND<100 <br /> Brornomethane ND<100 Methylene Chloride` ND<100 <br /> E n-Buiyl benzene ND<100 Methyl ethyl ketone" ND<100 <br /> sec-Butyl benzene ND<100 Methyi isobutyl ketoneND<100 <br /> tert-Butyl benzene ND<100 Methyi ten-Butyl Ether(MTBE) - <br /> • Carbon Disulfide ND<100 Napthalene ND<100 <br /> I Carbon Tetrachloride ND<100 n-Propyl benzene 110 <br /> Chlorobenzene ND<100 Styrene` ' ND<100 <br /> Chloroethane ND<100 1,1 12-Tetrachloroethane ND<100 <br /> 2-Chloroethyl Vinyl Ether"' ND<100 1 1 2 2-Tetiachloroethane ND<100 <br /> Chloroform ND<100 Tetrachlor❑etliene ND<100 <br /> Chloromethane ND<100 Toluene" 1900 <br /> 2-Chlorotoluene ND<100 1 2 3-Tnchiorobenzene ND<100 <br /> 4-Chlorotoluene ND<100 1 2 4-Trichlorobenzene ND<100 <br /> Dibromochloromethane ND<100 1,1 1-Trichloroethane ND<100 <br /> 12-Dibromo-3-chloropropane ND<100 1,12-Trichloroethane ND<100 <br /> Dibromomethane ND<100 rrichloroethene ND<100 <br /> 1,2-Dichlorobenzene ND<100 Trichlorotluoiomelhane ND<100 <br /> 1,3-Dichlorobenzene ND<100 1 2 3-Trichloropropane ND<100 <br /> 14-Dichlorobenzene ND<100 1,2 4-Trinethylbenzene 970 <br /> D=chlorodifluoromethane ND<100 1,3 5-Trimethylbenzene 350 <br /> 1,1-1])ichloroethane ND<100 Vinyl Acetate""' ND<100 <br /> I 12-Drehloroethane ND<100 Vinyl Chloride"" ND<100 <br /> f I i-Dichloroethene ND<100 Xylenes total `°' 4100 <br /> cis-1 2-Dichloroethene ND<100 <br /> E trans-12-Dichloroethene N13<100 <br /> I 2-Dtchloropropane ND<100 <br /> l 3-Dcchloropropane ND<100 <br /> 2,2-Dcchloropropane ND<100 Comments <br /> 1,1-Dtchloropropene ND<100 Surrogate Recoveries <br /> cis-1,3-Dichloropropene ND<100 Dibromofluoromethane 110 <br /> trans-13-Dichloropropene ND<100 Toluene-d8 100 <br /> Ethyiene dibromide ND<100 4-Biomof1uorobcnzcne 115 <br /> water and vapor samples are reported m ug/L,sod and sludge sampler in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 uglL n apor samples 0 5 ug/L, solid and sludge samples 5 ug/kg wipes <br /> 0 2ug/u,tpe ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-heaanone, (e) dichloromethane (f) 2-butanone, (g) 4-methyl-2- <br /> I pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present (i)liquid sample that contains greater than —5 vol % <br /> sediment,0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,(I)methylbenzene (m)acetic acid ethenyl ester (n)chlnroethene (o)dimethylbenzenes <br /> DHS Certification No 1644 // Edward Hamilton,Lab Director <br />