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i <br /> 110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> htW.//www.mccau2aell co m E-mail main@mccampbell com <br /> Advanced GeoEnviTonmental Client Project ID Cal Fuels Date Sampled 07116-07/17/98 <br /> 4005 North Wilson Way <br /> Date Received 07/22/98 <br /> Stockton,CA 95205 Client Contact Tun Cuellar Date Extracted 07/28/98 <br /> Client P O 7Date Analyzed 07/29-07/30/98 <br /> Oxygenated Volatile Organics By GC/MS <br />' EPA method 8260 modified <br /> Lab ID 92546 92547 92548 92549 <br /> MWl- MW2- MW3- MW4- Reporting Limit <br /> I Client ID 7/17198 7117/98 7/17/98 7/17/98 <br /> Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPE) ND<25 ND<250 ND<2000 ND<1000 50 10 <br /> Ethyl tert-Butyl Ether(ETBE) ND<25 ND<250 ND<2000 ND<1000 50 10 <br /> Methyl-tent Butyl Ether(MTBE) ND<25 ND<250 ND<2000 ND<1000 50 10 <br /> Itent-Amyl Methyl Ether(TAME) ND<25 ND<250 ND<2000 ND<1000 50 10 <br /> tert-Butanol ND<125 ND<1250 ND<10,000 ND<5000 25 50 <br /> I <br /> Surrogate Recoveries(%) <br /> Dibromofluoromethane 112 110 104 106 <br /> Comments J <br /> r water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> I <br /> DHS Certification No 1644 /4"1 Edward Hamilton Lab Director <br />