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I 10 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccampbeil com E-mail main@mccampbell com <br /> Advanced GeoEnvironmentalDate Sampled 07/01-03198 <br /> Client Project ID Cal-Fuels <br /> Date Received 07/09/98 <br /> 4005 North Wilson Way <br /> Stockton, CA 95205 Client Contact Tun Cuellar Date Extracted 07/10/98 <br /> I Client P O Date Analyzed 07/10/98 <br /> Volatile Organics By GCIMS <br /> EPA method 8260 <br /> Lab ID 91882 <br /> Client ID MW12-40 <br /> Matrix S <br /> Compound Concentration' Compound Concentration* <br /> Acetone` ' NIK50 Ethylbenzene ND <br /> Benzene ND Hexachlorobuladiene ND <br /> Bromobenzene ND lodomethane ND <br /> Bromochloromethane ND lsopropyl benzene ND <br /> Bromodichloromethane ND p-Isopropyl toluene ND <br /> Bromotorm ND Methyl butyl ketone' ' ND <br /> Bromomethane ND Methvlene C hioride"' ND<15 <br /> n-Butyl benzene ND Methyl ethyl ketone"' ND <br /> sec-Butyl benzene ND Methvl isobutyl Wone" ND <br /> tert-Butyl benzene ND Methyl ten-Butvl Ether(MTBE) <br /> Carbon Dtsulfide ND Naphthalene ND <br /> Carbon Tetrachloride ND n-Propyl benzene ND <br /> f hlorobenzene ND Styrene` ' ND <br /> Chloroethane ND I 1 12-Tetrachloroethane ND <br /> 2-Chloroethyl Vinyl Ether" ND 1 1 2 2-Tetrachloroethane ND <br /> Chloroform ND Tetrachloroethene ND <br /> Chloromethane ND Toluene" ND <br /> 2-Chlorotoluene ND 1 2 3-Trichlorobenzene ND <br /> 4-Chlorotoluene ND 1 2 4-Ti chlorobenzene ND <br /> DSbCOmOChlOTOmelhane ND 1 l 1-Trichloroethane ND <br /> l2-Dibromo-3-chloropropane ND I 12-Trichloroethane ND <br /> Dibromontethane ND Trichloroethene ND <br /> I2-Dichlorobenzene ND Tnchlorolluorontethane ND <br /> I 3-Dichlorobenzene ND 1 2 3-Trichloropropane ND <br /> I 4-Dichloroben2ene ND 1 2 4 Trimethylbenzene ND <br /> Dichlorodifluoromethane ND 1 3 5 Ti i methy]benzene ND <br /> I l-Dichloroethane ND Vin)I Acetate"" ND <br /> I 2-Dichloroethane ND Vinyl Chloride"" ND <br /> 1,1-Dichloroethene ND Xvlenes total '°' ND <br /> cis-] 2-Diebloroetbene ND <br /> trans-] 2-Dichloroethene ND <br /> 12-Dichloropropane ND <br /> 13-Dichloropropane ND <br /> 2 2-Dichloropropane ND Comments <br /> 1 I-Dichloropropene ND Surrogate Recoseries('%.) <br /> cis-1,3-Dichloropropene ND Dibromoiluoromethane 102 <br /> trans-1,3-Dichloropropene ND Toluene-d8 107 <br /> Ethylene dibromide ND 4-Brornot11.101oberizenc 98 <br /> water and vapor samples are reported to ug/L soil and sludge samples to tig/kg,A%ipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 uglL s apor samples 0 5 uglL suhd and siudge samples 5 ug/kg, wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone (e) dichloromethane (f) 2-butanone, (g) 4-methyl-2 <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present (i)liquid sample that contains greater than —5 vol % <br /> sediment,0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard fol <br /> this analyte,(1)methylbenzene (m)acetic acid ethenyl ester,(n)chloroethenc (o)dimer ylbenzenes <br /> DHS Certification No 1644 / Edward Hamilton, Lab Director <br />