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ld <br /> 110 2rld Avcntic Sla11lh,II[)7, Pacheco,C>'1 945534560McCAN11'I LL ANALYTICAL INC, `�'CICPI'anc�925-798.1620 Fax:925-798-1022 <br /> http://www.mccampbcll.com E-mail: main@amccatnpbell.com <br /> Advanced GeoEnvirorimental Client Project ID: Cal Fuels Date Sampled: 10/29-30/01 <br /> 837 Shaw Road Date Received. 10/31/01 <br /> Stockton,CA 95215 Client Contact: Tim Cuellar Date Extracted: 11/03/01 <br /> Client P.O: Date Analyzed: 11/03/01 <br /> EPA method 8260 Volatile Organics By GC/MS <br /> Lab M 82294 <br /> Client ID CPT-1/131-136 <br /> Matrix W <br /> Compound Concentration' Repomng Limn * Reporting Limit <br /> P W S �C�ompound Concentration <br /> W S <br /> Acetone(b) ND SA q25trans-1,3-Dichloropropene ND 1.0 5.0 <br /> &' Benzene ND 1.0 Ethyiene dibromide ND I.0 5.0 <br /> Bromobenzene ND 1.0 Ethylbenzene ND 1.0 5.0 <br /> Bromocftloromethane ND 1.0 5.0 Hexachlorobutadiene ND 5.0 25 <br /> Bromodichloromethane ND 1.0 5.0 iodomethane ND 1.0 5.0 <br /> Bromoform ND 1.0 5.0 lsopropyibenzene ND 1.0 5.0 <br /> Bromomethane ND 1.0 5.0 p-isopropyi toluene ND 1.0 5.0 <br /> n-Butyl benzene ND 1.0 5.0 Methyl butyl ketone t ND 1.0 5.0 <br /> sec-Butyl benzene ND 1.0 5.0 Methylene Chloride'J ND 1.0 5.0 <br /> tert-Butyl benzene ND 1.0 5.0 Methyl ethyl ketone ND 2.0 10 <br /> Carbon Disulfide ND 1.0 5.0 Methyi isobutyl ketone ND 1.0 5.0 <br /> Carbon Tetrachloride ND 1.0 5.0 Methyl tert-Butyl Ether(MTBE) - 1.0 5.0 <br /> Chlorobenzene ND 1.0 5.0 Naphthalene ND 5.0 5.0 <br /> Chloroethane ND l.0 5.0 n-Propyl benzene ND 1.0 5.0 <br /> 2-Chloroethyi Vinyl Ether` ND 1.0 5.0 Styrenes ND 1.0 5.0 <br /> Chioroform ND 1.0 5.0 1,1,1,2-Tetrachloroethane ND 1.0 5.0 <br /> 160 Chioromethane ND LO 5.0 1,1,2,2-Tetrachloroethane ND 1.0 5.0 <br /> 2-Chlorotoluene ND 1.0 5.0 Tetrachloroethene ND 1.0 5.0 <br /> 4-Chlorotoluene ND 1.0 5.0 Toluene 1.4 1.0 5.0 <br /> Dibromochioromethane ND 1.0 5.0 1,2,3-Trichlorobenzene ND 5.0 25 <br /> i. 1,2-Dibromo-3-chloropropane ND 2.0 10 1,2,4-Trichlorobenzme ND 5.0 25 <br /> Dibromomethane ND 1.0 5.0 1,1,1-Trichloroethane ND 1.0 5.0 <br /> 1,2-Dichlorobenzene ND 1.0 5.0 1,1,2-Trichloroethane ND 1.0 5.0 <br /> 1,3-Dichlorobenzene ND 1.0 5.0 Trichloroethene ND 1.0 5.0 <br /> a� 1,4-Dichlorobenzene ND 1.0 5.0 Trichlorofluoromethane ND 1.0 5.0 <br /> Dichlorodifluoromethane ND 1.0 5.0 1,2,3-Trichloropmpane ND lA 5.0 <br /> 1,1-Dichloroethane ND 1.0 5.0 1,2,4-Trimethylbenzene ND 1.0 5.0 <br /> 1,2-Dichloroethane ND 1.0 5.0 1,3,5-Trimethylbenzene ND 1.0 5.0 <br /> 1,1-Dichloroethene ND 1.0 5.0 Vinyl Acetate m ND 5.0 25 <br /> cis-1,2-Dichloroethene ND 1.0 5,0 Vinyl Chloride ° ND 1.0 5.0 <br /> trans-1,2-Dichloroethene ND 1.0 5.0 Xylenes,total `° ND 1.0 5.0 <br /> 1,2-Dichloropropane ND 1.0 5.0 Comments: <br /> 1,3-Dichloropropane ND 1.0 5.0 Surrogate Recoveries(%) <br /> 2,2-Dichlaropropane ND 1.0 5.0 Dibromofluoromethane 106 <br /> 1,1-Dichloropropene ND 1,0 5.0 Toluene-d8 100 <br /> cis-1,3-Dichloropropene ND 1.0 S.0 4-Bromofluoroben7ene 96 <br /> Lr water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means analyte not applicabie to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> V pentanone or isopropylacetone; (h) lighter than water immiscible sheen is present; (i) liquid sample that contains greater than--5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; 0) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br /> V <br /> L <br />