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1 I 0 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br />' 4 MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//wwwmccampbelleo E-rriail main@mccampbell com <br /> • <br /> Advanced GeoEnvironmental Client Project ID Cal Fuels Date Sampled 08/16/00 <br /> 4005 North.Wilson Way Date Received 08/25/00 <br /> 1 Stockton, CA 95205 Client Contact Tim Cuellar Date Extracted 08/25/00 <br />' Client P O Date Analyzed 08/25-08/28/00 <br /> 7 Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br />' Lab 1D 45880 <br /> Reporting Limit <br /> Client ID MW 13-95 <br />' Matrix S S W <br /> Compound Concentration* ug/kg ug/L <br />' Di-isopropyl Ether(DIPS) ND 50 1 1 0 <br /> Ethyl tert-Butyl Ether(ETBE) ND 50 10 <br /> Methyl-tert Butyl Ether(MTBE) ND 50 to <br />' . tert-Amyl Methyl Ether(TAME) ND 50 10 <br /> tert-Butanol ND 25 50 <br />' Methanol ND 1000 200 <br /> Ethanol ND 250 50 <br /> Surrogate Recoveries{%) <br /> Dibromofluoromethane 92 <br /> Comments <br /> K. <br /> "water samples are reported in n <br /> p p g/1.,soil and sludge samples in wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,NIA means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,(1)sample diluted due to <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />