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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br />' McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> h_ttp//www mccampbell com E-mail main@mccampbell com <br />' Advanced GeoEnvironmental Client Project ID Cal Fuels Date Sampled 09/12/00 <br /> 4005 North Wilson Way Date Received 09/19/00 <br /> Stockton, CA 95205 Client Contact Tim Cuellar Date Extracted 09/25-09/27/00 <br /> Client P O Date Analyzed 09/25-09/27/00 <br /> 7 Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab 1D 47855 <br /> MW 13/09- Reporting Ltrrut <br /> Client 1D 12-00 <br /> Matrix W S W <br /> Compound Concentration* Ug/kg ug/L <br /> I Di-isopropyl Ether(D1PE) ND <br /> 50 1 0 <br /> Ethyl tert-Butyl Ether(ETBE) ND 50 1 0 <br />( � Methyl-tert Butyl Ether(MTBE) ND<3 5 50 1 1 0 <br /> tert-Amyl Methyl Ether(TAME) ND 50 1 0 <br /> text-Butanol ND 25 50 <br /> Methanol ND<20,000 1000 200 <br /> IEthanol 1$0,000 250 50 <br /> Surrogate Recovenes(%) <br /> Dibromofluoromethane 94 <br />� %ummenrs <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wmpe and all TCLP 1 STLC/SPLP extracts to ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysts <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> r <br /> lugh organic content <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />