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1 1 1102nd Avenue South,#D7 Pacheco,CA 94553 5560 <br /> McCampbell Analytical Inc Telephone 925 798-1620 Fax 925-798-1622 <br /> h l/www mccaiigaliell com E mail mam mccarrnpbell com <br /> Advanced GeoEnvironmental, Inc Client Project ID Cal Fuels Date Sampled 06/24/03 <br /> 837 Shaw Road Date Received 06/25/03 <br /> Client Contact Tim Cuellar Date Extracted 06128103-07101103 <br /> Stockton,CA 95215 <br /> Client P O Date Analyzed 06/28103-07101103 <br /> Oxygenated Volatile Organics+EDB and 1,2-DCA by P&T and GC/MS* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0306526 <br /> Lab 1D 0306526-0018 0306526-002B 0306526-003B 0306526-004B <br /> Client ID MW1 MW2 MW3 MW4 <br /> � Reporting Limit for <br /> Matrix W fly W W DF=1 <br /> DF I I T-s W <br /> Compound Concentration ug/kg µg/L <br /> Dusopropyl ether(DUPE) ND ND ND ND<2 5 NA 05, <br /> Ethyl tert-butyl ether(ETBE) ND ND ND ND<2 5 NA 05 <br /> Methyl-t-butyl ether(MTBE) ND ND ND ND<2 5 NA 05 <br /> tert-Amyl methyl ether(TAME) ND ND ND ND<2 5 NA 05 <br /> t-Butyl alcohol(TBA) ND ND 14 ND<25 NA 50 <br /> 1,2-Dtbromoethane(EDB) ND ND ND ND<2 5 NA 05 <br /> 1,2-Dichloraethane(1,2-ACA) ND ND 49 ND<2 5 NA 05 <br /> Surrogate Recoveries(%) <br /> %SS 114 113 112 105 <br /> Comments h <br /> *water and vapor samples and all TCLP&SPLP extracts are reported to 14g/1, soil/sludge/solid samples inµg/kg, wipe samples inµg/wipe, <br /> product/all/non-aqueous liquid samples to mg/L. <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> hl lighter than water tmmwcihle sheen/tirnduct is nresent it houid sample that contains greater than—2 vol %sediment 1)sample diluted due to h1_eh <br /> organic content ✓ <br /> DHS Certification No 1644 Angela Rydehus, Lab Manager <br />