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I <br /> rt 110 2nd Avenue South t1D7 Pacheco CA 94553-5560 <br /> LAO McCampbell Analytical Inc Telephone 925-798-1620 Fax 925-798 1622 <br /> http//www ince bell corn E-mail inainQuiccanilibell corn <br /> Advanced GeoEnvironmental,Inc Client Project ID Cal Fuels Date Sampled 06/24/03 <br /> 837 Shaw Road <br /> Date Received 06/25/03 <br /> Stockton,CA 95215 Client Contact Tim Cuellar Date Extracted 06128/03-07101/03 <br /> Client P O Date Analyzed 06/28/03-07101/03 <br /> I <br /> Oxygenated Volatile Organics+EDB and 1,2-DCA by)P&T and GC/MS* <br /> Extraction Method SW50308 Analytical Method SW8260B Work Order 0306526 <br /> Lab ID 0306526-009B 030656-010130306526-011B 0306526-012B <br /> Client ID MW9 MW10 MWI l MW12 <br /> Reporting Limit for <br /> Matnx W W W W DF=1 <br /> Compound Concentration ug/kg µg/L <br /> Dusopropyl ether(DIP$) ND ND ND ND NA 05 <br /> Ethyl tert-butyl ether(ETRE) ND ND ND ND NA 05 <br /> Methyl-t-butyl ether(MTBE) ND ND ND ND NA 05 <br /> tert-Amyl methyl ether(TAME) ND ND ND ND NA 0 5 <br /> t-Butyl alcohol(TBA) ND ND ND ND NA 50 <br /> 1,2-Dibromoethane(EDB) ND ND ND ND NA 05 <br /> 1,2-Dichloroethane(1,2-DCA) ND ND ND ND NA 05 <br /> Surrogate Recoveries(%) <br /> —7 <br /> %SS 115 114 117 117 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in gg/L,soiVsludge/solid samples to pg/kg, wipe samples In pg/wipe <br /> product/oil/non-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present i)liquid sample that contains greater than—2 vol %sediment 0 sample diluted due to hrQ_h <br /> or ante content <br /> DHS Certification No 1644 Angela Rydelius, Lab Manager <br />