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+ 110 2nd Avenue South,4D7,Pacbecn,CA 94553-5560 <br /> McCampbell Analytical Tic Telephone 925-798-1620 Fax 925-798-1622 <br /> h /lwww mccarripbell cam E mail mTp a mecanpbell coin <br /> Advanced GeoEnvironmental,Inc Client Project ID Cal Fuels Date Sampled 06/24/03 <br /> 837 Shaw Road Date Received 06/25/03 - <br /> Client Contact Tim Cuellar Date Extracted 06128/03-07/01103 <br /> Stockton,CA 95215 <br /> Client P O Date Analyzed 06/28/03-07101/03 <br /> Oxygenated Volatile Organics+EDB and 1,2-DCA by P&T and GC/MS* <br /> Extraction Method SW503013 Analytical Method SW8260B Work Order 0306526 <br /> Lab ID 0306526-017B 0306526-018B 0306526-019B <br /> CltentID AW1B AW2A AW2B <br /> Reporting Limit for <br /> Matrix W W1 <br /> DF=I <br /> DF 5 100 -------�--- <br /> -__ S W <br /> Compound Concentration ug/kg pg/L <br /> Diisopropyl ether(DIPE) ND<2 5 ND<50 ND NA 0 5 <br /> Ethyl tert-butyl ether(E7 BE) ND<2 5 ND<50 ND NA 0 5 <br /> Methyl-t-butyl ether-(MTBE) ND<2.5 ND<50 053 NA 05 <br /> tert-Amyl methyl ether(TAME) ND<2 5 ND<50 ND NA 05 <br /> t-Butyl alcohol(TSA) ND<25 ND<500 ND NA 50 <br /> 1,2-Dibromoethane(EDB) ND<2 5 ND<50 ND NA 0 5 <br /> 1,2-Dichloroethanc(1,2-DCA) 34 ND<50 41 NA 0 5 <br /> Surrogate Recoveries(%) <br /> %SS 105 982 106 <br /> Comments j <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in gg/L,soil/sludge/solid samples in gg/kg, wipe samples in pg/wtpe, <br /> product/oil/non-aqueous liquid samples in mg/L. <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,l)sample diluted due to high <br /> or anic content <br /> i - <br /> DHS Certification No 1644 Angela Rydebus,Lab Manager <br />