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S <br /> 110 2nd Avenue South,4D7,Pacheco,CA 94553-5560 j <br /> McCampbell Analytical Inc. Telephone:925-798-1620 Fax:925-798-1622. G <br /> ' hrtpalwww.mcrampbell.com E-mail:mam@mcrampbelLcom <br /> C SUMMARY REPORT FOR SW8021S/8015Cm Ir <br /> I . <br /> Matrix:W WorkOrder: 0209369 <br /> EPA Method: SW8021 B18015CM Extraction: SW5030B Batch ID:4111 Spiked Sample ID: NIA <br /> Sample Spiked MS" MSD' MS-MSD'i LCS �, LCSD ILCS-LCSDAcceptance Criteria(/°) <br /> o <br /> i P I' - - -- - <br /> Compound = — - -- <br /> �IglL �pgIL %Rec. �i %Rec. I-%RPD ` %Rec. %Rec. i %RPD Low High <br /> - — -NIA 112 110- 2,00, 8U 120 <br /> NIA 60 N/A NIA <br /> i <br /> TPH{gas) <br /> MTBF NIA 10 N/A NIA N/A 101 —108 6.95 y 80, i 120 <br /> Benzene NIA 10 NIA NIA N/A 99 105 6.25' 80, 120 <br /> --- <br /> a Toluene NIA 10 NIA N/A NIA I 102 109 } 6.60 i 80: 120 <br /> Eth lbenzene - NIA to N/A NIA NIA 106 110 i 3.10.; 803 120 <br /> Xylenes NIA 30 NIA N/A NIA 103 107 3.17 80 120 <br /> NIA i 100 NIA N/A NIA 95.5 96.4 0.941, 80 320 <br /> All target compounds in the Method Blank of'this extraction batch were ND less than the method KL with the following exceptions: .. <br /> NONE <br /> F <br /> r <br /> a <br /> i r <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent <br /> Deviation. <br /> NIA=not enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due td high matrix or j <br /> analyte content. + <br /> %Recovery=100'(MS-Sample)1(Amount Spiked);RPD=100'(MS-MSD)/(MS+MSD)'2. <br /> "MS and/or MSD spike recoveries may not be near 100%or the RPDs near 0%if:a)the sample is inhomogenous AND contains significant concentrations of <br /> analyte relative to the amount spiked,or b)if that specific sample matrix interferes with spike recovery. <br /> i <br />