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CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive,Atwater,CA 95301 Phone (209)384-2930 <br />' Certificate No 2480 Fax (209)384-1507 <br /> Advanced GeoE nviron mental Inc Client Project ID Cal Fuels Sampled 06-20-02 <br />' of Northern California Reference Number 4805 Received 06-21-02 <br /> 837 Shaw Road Sample Description Water Extracted 06-27-02 <br /> Stockton,CA 95215 Sample Prep/Analysis Method EPA 5030/8260 Analyzed 06-27-02 <br /> Attn Tim Cuellar Lab Numbers 4805-6W, 7W,8W,9W, 10W Reported 07-08-02 <br /> GASOLINE ADDITIVES BY EPA METHOD 8260 GCIMS <br />' ANALYTE REPORTING SAMPLE ID SAMPLE ID SAMPLE ID SAMPLE ID SAMPLE ID <br /> LIMIT MW 6 MW 7 MW 8 MW 9 MW 10 <br />' 062002 062002 062002 062002 062002 <br /> /L u IL (Ug/L (ug/L (ug/L (UWL) <br /> FUEL OXY,CENATES <br />' Methyl tert-Butyl Ether(MTBE) 050 NO ND NO ND ND <br /> Di-isopropyl Ether (DIPE) 0 50 NO ND ND NO ND <br />' Ethyl tert-Butyl Ether (ETBE) 050 NO NO ND ND ND <br /> tert-Amyl Methyl Ether(TAME) 0 50 NO NO ND ND ND <br /> Itert-Butanol(TBA) 20 Nil NO ND NO ND <br />' VOLATILE HALOCARBONS <br /> 1 2-Dichloroethane (1,2-DCA) 0 50 ND NO NO NO ND <br />' Ethylene Dibromide (EDB) 050 ND NO NO ND NO <br /> Report Limit Multiplication Factor 1 1 1 1 1 <br /> C�rrnnatp F7ornvoriac <br /> 1,2-Dichloroethane-d4 101% 984% 103% 100% 988% <br />' Toluene-d8 105% 989% 104% 104% 990% <br /> Instrument ID Varian Saturn 3&HP 5972 MS <br /> Analytes reported as NO were not detected or below the Practical Quantitation Limit <br /> Practical Quantitation Limit=Reporting Limit x Report Limit Multiplication Factor <br />' (Ng/L)= micrograms per liter or parts per billion(ppb) <br />' ANALYST APPROVED BY ge�x—�l <br /> Clan J Cone JanjAX C Phillips <br /> oratory Director <br />