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CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive,Atwater, CA 95301 Phone (209)384-2930 <br />' Certificate No 2480 Fax (209)384-1507 <br /> Advanced GeoEnvironmental, Inc Client Project ID Cal Fuels Sampled 06-20-02 <br />' of Northern California Reference Number 4805 Received 06-21-02 <br /> 837 Shaw Road Sample Description Water Extracted 06-27-02 <br /> Stockton,CA 95215 Sample Prep/Analysis Method EPA 5030/8260 Analyzed 06-27-02 <br /> Attn Tim Cuellar Lab Numbers 4805-16W Reported 07-08-02 <br /> I <br /> GASOLINE ADDITIVES BY EPA METHOD 8260 GC/MS <br />' ANALYTE REPORTING SAMPLE ID <br /> LIMIT AW 2B <br />' 062002 - - — <br /> (Ng/L) (u91L) <br /> FUEL OXYGENATES <br />' Methyl tert-Butyl Ether(MTBE) 050 ND <br /> Di-isopropyl Ether (DIPE) 050 ND <br /> Ethyl tert-Butyl Ether (ETRE) 050 ND <br /> Ile tert-Amyl Methyl Ether(TAME) 050 ND <br /> tert-Butanol(TBA) 20 ND <br /> IV LAT CARBON <br /> 1,2-Dichloroethane (1,2-DCA) 050 ND <br /> Ethylene Dibromide (EDB) 050 ND <br /> IReport Limit Multiplication Factor 50' <br /> I <br /> I *Re ort limit raised due to matnx interference <br /> Siirmnnale 12Prnvariac <br /> 1 2-Dichloroethane-d4 680% <br /> I Toluene-d8 106% <br /> Instrument ID Varian Saturn 3&HP 5972 MS <br /> Analytes reported as ND were not detected or below the Practical Quantitation Limit <br /> Practical Quantitation Limit= Reporting Limit x Report Limit Multiplication Factor <br /> I (Ng/L)= micrograms per liter or p billion(ppb) <br /> r <br /> I ANALYST APPROVED BY <br /> CI J Cone Ja s Phillips <br /> aboratory Director <br /> I <br />