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' CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive,Atwater, CA 95301 Phone (209)3842930 <br />' Certificate#2480 Fax (209)3841507 <br /> Advanced GeoEnvironmental, Inc Client Project ID Cal Fuels(Pacific) Sampled 03-08-02 <br />' of Northern Caldomm Reference Number 4487 Received 03-12-02 <br /> 837 Shaw Road Sample Description Water Extracted 03-15-02 <br /> Stockton, CA 95215 Sample Prep/Analysis Method EPA 5030/8260 Analyzed 03-15-02 <br /> Attn Tim Cuellar Lab Numbers 4487-1W,2W,3W,4W, 5W Reported 03-22-02 <br /> GASOLINE ADDITIVES BY EPA METHOD 8260 GUMS <br />' ANALYTE REPORTING SAMPLE ID SAMPLE ID SAMPLE ID SAMPLE ID SAMPLE ID <br /> LIMIT MW 1 MW 2 MW 3 MW 4 MW 5 <br />' 030802 030802 030802 030802 030802 <br /> -- (h5/L) (ug/L) (ug/L)- --- (ug/L) (ug/L) (ug/L) . <br /> FUEL OXYGENATES <br />' Methyl tert-Butyl Ether(MTBE) 0 50 ND ND ND ND 065 <br /> Di-isopropyl Ether (DIPE) 050 ND ND ND ND ND <br /> Ethyl tert-Butyl Ether (ETBE) 050 ND ND ND NO ND <br /> tert-Amyl Methyl Ether(TAME) 050 ND ND ND ND ND <br /> lie tert-Butanol(TBA) 20 ND ND ND ND ND <br /> 1 <br /> Report Limit Multiplication Factor 1 1 50* 20" 1 <br /> 1 <br /> 1 <br /> "Dilution required due to matrix interference <br /> C�rrn�7jfa Rarn�enae <br /> 1,2-Dichloroethane-d4 899% 91 8% 894% 905% 932% <br />' Toluene-0 105% 127% 970% 906% 943% <br /> Instrument ID Varian Saturn 3 <br /> Analytes reported as ND were not detected or below the Practical Quantitation Limit <br /> Practical Quantitation Limit=Reporting Limit x Report Limit Multiplication Factor <br /> (pg/L)= microgr s er titer o pe billion(ppb) <br /> ANALYST APPROVED BY Of A Z�41 <br /> I Clan J Gone Ja s turps <br /> L oratory Director <br /> I <br />