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1 <br /> 110 2nd Avenue South #D7 Pacheco CA 94553 X560 <br /> McCampbell Analytical Inc Telephone 925 798 1620 Fax 925-798 1622 <br /> [:A:#' http//www mccarripbell com E mail rmin@mccarnpbell com - <br /> Advanced GeoEnvirorimental, Inc Client Project ID Arco Pacific Mini Mart Date Sampled 11/26/02 <br />' 837 Shaw Road Date Received 11/27/02 <br /> Stockton, CA 95215 Client Contact Bill Little Date Extracted 12/03/02-12/06/02 <br />' Client P O Date Anaiyzed 12/03/02-12/06102 <br /> Oxygenated Volatile Organics by P&T and GC/MS* <br /> Extraction Method SW503013 Analytical Method SW8260B Work Order 0211472 <br />' Lab ID 0211472-009C 0211472-010C i 0211472-011C 0211472-012C <br /> Client 1D MW9 M W 10 I MW l i A MW I I B Reporting Limit for <br />' Matrix W W i W W DF=1 <br /> -- - -- --- - ---- — - - - -- - --1 _ -- - -- - <br /> DF 1 1 40 10 S W <br /> I I <br /> Compound Concentration ng/kg µg/L <br /> Dusopropyl ether(DIPS) ND ND ND<20 ND<5 0 NA 05 <br />' Ethyl tert-butyl ether(ETRE) ND ND ND<20 ND<5 0 NA 05 <br /> Methyl-t-butyl ether(MTBE) ND ND 640 190 NA 0 5 <br /> tert-Amyl methyl ether(f AME) ND ND ND<20 ND<5 0 NA 05 <br /> It-Butyl alcohol(TBA) ND ND ND<200 ND<50 NA 50 <br /> IMethanol ND ND ND<20,000 ND<5000 NA 500 <br /> Ethanol ND ND NDQ000 ND<500 NA 50 <br /> I1,2-Dibromoethane(EDB) ND ND ND<20 ND<5 0 NA 05 <br /> 1,2-Dichtoroethane(1,2-DCA) ND ND ND<20 ND<5 0 NA 05 <br /> tSurrogate Recoveries(%) <br /> I %SS F 1: 105 107 104 106 <br /> — — — J <br /> Comments <br /> i i <br /> *water and vapor samples and all TCL.P&SPLP extracts are reported in}tg/L,soil/sludge/solid samples inµg/kg, wipe samples in ug/wtpe, <br /> product/oil/non-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> I h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than-2 vol %sediment,j)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />