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I�2.denue South,ti07Pacheco,CA 94553-5560 McCampbell Analytical Inc ne9Z5-798-1620 Fax 925-798-1622 pcamphell com E-mail mai r@mccampbell com Advanced GeoEnvironinental Client Project ID Pacific Mini Mart Date Sampled 05/13/02 837 Shaw Road Date Received 05/14/02 Stockton,CA 95215 Client Contact Bill Little Date Extracted 05/14/02 Client P O Date Analyzed 05/16/02 Semi-Volatile Organics by GC/MS(625 Basic Target List)* Extraction Method SW351oC Analytical Method SW8270D Work Order 0205187 Lab ID 0205187-003D Client ID Effluent Matrix Water Compound Concentration * Dl: ft`Pc°ma,�s Compound Concentration * DF R= Acenaphthene ND 1 0 10 Acenaphthylene ND 10 10 Anthracene ND 10 10 Benzidine ND 10 10 Benzoic Acid ND 1 0 50 Benz(a)anthracene ND 1 0 10 Benzo(b)fluoranthene ND 10 10 Benzo(k)fluoranthene ND 10 10 Beazo(g,h,t)peryiene ND 1 0 10 Benzo(a)pyrene ND 10 10 Benzy]Alcohol ND 1 0 20 Bis(2-chlormthoxy)Methane ND 10 10 Bis(2-chloroethyl)Ether ND 1 0 10 Bis(2-chloroisopropyl)Ether ND 10 10 Bis(2-ethylhexyl)Phthalate ND 1 0 10 4-Bmmophenyl Phenyl Ether ND 1 0 10 Butylbenzyl Phthalate ND 1 0 10 4-Chloreaniline ND 10 10 4-Chloro-3-methylphenol ND 10 10 2-Chloronaphthalene ND 10 10 2-Chlorophenol ND 1 0 10 4-Chlomphenyl Phenyl Ether ND 10 10 Chrysene ND 1 0 10 Dibenzo(a,h)anthracene ND 10 10 Dibenzofuian ND 1 0 10 Di-n-butyl Phthalate ND 10 10 1,2-Dichlorobenzene ND 10 10 1,3-Dichlorobenzene ND 10 10 1,4-Dichlorobenzene ND 10 10 3,3-Dichlorobenz3dine ND 10 20 2,4-Dichlorophenol ND 1 0 10 Diethyl Phthalate ND 1 0 10 2,4-Dimethylphenol ND 1 0 10 Dtmethyl Phthalate ND 1 0 10 4,6-Dinitro-2-methylphenol ND 10 50 2,4-Dmitrophenol ND 10 50 2,4-Dmitrotoluene ND 10 10 2,6-Dmitrotoluene ND 10 10 Di-n-octyl Phthalate ND 1 0 10 1,2-Diphenylhydrazine ND 1 0 10 Fluoranthene ND 10 10 Fluorene ND 10 10 Hexachlorobenzene ND 10 10 Hexachlorobutadiene ND 10 10 I Hexachlomcyclopentadiene ND 10 10 Hexachloroethane ND 10 10(1,2,3--ed)Indeno(1,2,3d)pyrene ND 1 0 10 Isophorone ND 1 0 10 2-Methylnaphthalene ND 1 0 10 2-Methylphenol(o-Cresol) ND 1 0 10 3&/or 4-Methylphenol(m,p-Cresol) ND 1 0 10 Naphthalene ND 1 0 10 2-Nitroanilme ND 1 0 10 3-Nitroaniline ND 10 50 4-Nitroamline ND 1 0 10 2-Nitrophenol ND 10 10 4-Nitrophenol ND 1 0 10 Nitrobenzene ND 1 0 50 N-Nitrosodiphenylamine ND 10 10 N-Nitrosodi-n-propylamine ND 10 10 ' Pentachlorophenol ND 10 10 Phenanthrene ND 10 50 Phenol ND 10 10 Pyrene ND 10 10 1,2,4-Triehlorobenzene ND 10 10 2,4,5-Trichlorophenol ND 10 10 2,4,6-Tnebloro henol ND 1 0-1-10 Surrogate Recoveries(°/a) 411 %JJL J6 1 %SS3 501 %SS4 537 %SS5 443 %SS6 541 ' Comments *water and vapor samples and all TCLP&SPLP extracts are reported in ug/L.,soil and sludge samples in mg/kg, wipe samples in ug/wipe,olUnon- aqueous liquid samples in mg/L ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis #surrogate diluted out of range or surrogate coelutes with another peak h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than–2 vol %sediment,j)sample diluted due to high organic content DHS Certification No 1644 Edward Hamilton,Lab Director