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I 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 ' http l/www mccampbell co m E-mail main@mccampbell com ' Advanced GeoEnvironmental Client Project ID Pacific Mini Mart Date Sampled 04/22/02 837 Shaw Road Date Received 04/23/02 ' Stockton, CA 95215 Client Contact Bill Little Date Extracted 04/23/02 Ghent P O Date Analyzed 04/23-04/24/02 Copper and the LUFT Metals* EPA analytical methods 6010/200 7,239 2� Lab CD Client 1D Matrix Exttactton° Cadmium Chromium Copper Lead Nickel Zinc u Rg Surrogate ' 0204360 EFFLUENT W TTLC ND ND ND ND ND ND 108 -002 I f lie S TTLC 0 5 mg/kg 05 2 0 30 20 10 Reporting Limit unless ' otherwise stated,ND means W TTLC 0 005 mg/L 0 02 0 05 0 005 0 OS 0 OS not detected above the reporting limit ___ STLC, TCLP 0 01 mg/L 005 005 02 005 005 *water samples are reported in mg/L,soil and sludge samples to mg/kg,wipes in ug/wipe and all TCLP I STLC I SPLP extracts in mg/L "Lead is analysed using EPA method 6010(ICP)for soils,STLC&TCLP extracts and method 239 2(AA Furnace)for water samples °EPA extraction methods 1311(TCLP),301013020(water,TTLC),3040(organre matrices,TTLC),3050(solids,TTLC),STLC-CA Title 22 DiSTLC extractions are performed using STLC methodology except that deionized water is substituted for citric acid buffer as the extraction fluid DISTLC results are not applicable to STLC regulatory limits Surrogate diluted out of range,N/A means surrogate not applicable to this analysis I &reporting limit raised due to matrix interference i) liquid sample that contains greater than --2 vol % sediment, this sediment is extracted with the liquid, in accordance with EPA methodologies and can significantly effect reported metal concentrations DHS Certification No 1644 Edward Hamilton,Lab Director