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110 Second Avenue South,#fD7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />' 24 hmiJ/www mccamnbell com E-mail main@mecampbell corn <br /> Date Sampled 06/15/98 <br /> Advanced GeoEnvironmental Client Project ID #0128,Arco <br /> Date Received 06/17/98 <br /> 4005 North Wilson Way <br /> Stockton,CA 95205 Client Contact Bill Little Date Extracted 06/20/98 <br /> Client P O Date Analyzed 06/20/98 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 90592 <br /> Client ID VW1/6-15-98 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br />' Acetone ND<140 Ethylbenzene 1800 <br /> Benzene 280 Hexachlorobutadiene ND<100 <br /> Bromobenzene ND<100 Iodomethane ND<100 <br /> Bromochloromethane ND<100 Isopropylbenzene ND<100 <br />' Bromodichloromethane ND<100 p-Isopropyl toluene ND<100 <br /> Bromoform ND<100 Methyl butyl ketone ND<100 <br /> Bromomethane ND<100 Methylene Chlonde` ND<100 <br /> n-Butyl benzene ND<100 Methyl ethyl ketone ND<100 <br />' sec-Butyl benzene ND<100 Methyl isobutyl ketones ND<100 <br /> tert-Butyl benzene ND<100 Methyl tert-Butyl Ether(MTBE) <br /> Carbon Disulfide ND<100 Naphthalene ND<620 <br /> Carbon Tetrachloride ND<100 n-Propyl benzene ND<100 <br /> Chlorobenzene ND<100 Styrene ND<100 <br /> Chloroethane ND<100 1,1,1,2-Tetrachloroethane ND<100 <br /> 2-Chloroethyl Vinyl Ethe ND<100 1,1,2,2-Tetrachloroethane ND<100 <br /> Chloroform ND<100 Tetrachloroethene NIx100 <br />' Chloromethane ND<100 Toluene 2100 <br /> 2-Chlorotoluene ND<100 1,2,3-Tnchlorobenzene ND<100 <br /> 4-Chlorotoluene NIX 100 1,2,4-Tnchlorobenzene ND<100 <br /> Dibromochloromethane ND<100 1,1,1-Trichloroethane ND<100 <br />' 1,2-Dibromo-3-chloropropane ND<100 1,1,2-Tnchloroethane ND<100 <br /> Dibromomethane ND<100 Tnchloroethane ND<100 <br /> 1,2-Dichlorobenzene ND<100 Tnchlorofluoromethane ND<100 <br /> 1,3-Dichlorobenzene ND<100 1,2,3-Tnchloropropane ND<100 <br />' 1,4-Dichlorobenzene ND<100 1,2,4-Tnmethylbenzene 2900 <br /> Dichlorodifluoromethane ND<100 1,3,5-Trimethylbenzene 880 <br /> ],1-Dichloroethane ND<100 Vinyl Acetate "' ND<100 <br /> 1,2-Dichlomethane ND<100 Vinyl Chloride " ND<100 <br /> 1,1-Dichloroethene ND<100 Xylenes,total `° 7800 <br /> cis-1,2-Dichloroethene ND<100 <br /> trans-] 2-Dichloroetbene ND<100 <br /> 1,2-Diehl oropropane ND<100 — <br /> 1,3-Dichloropropane N DE100 <br /> 2,2-Dichloropropane ND<100 Comments <br /> IJ-Dichloropropene ND<100 Surrogate Recoveries(%) <br />' cis-1,3-Dichloropropene ND<100 Dibromofluoromethane 113 <br /> trans-],3-Dichloropropene ND<100 Toluene-d8 103 <br /> Ethylene dibromide ND<100 4-Bromofluorobenzene 99 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L, vapor samples 0 5 ug/L, solid and sludge samples 5upi/kg, wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis a _ <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanonc, (e) dichloromethane, (f) 2butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than,-5 vol % <br /> sediment,0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattem of our standard for <br /> this analyte,p)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 /4 Edward Hamilton,Lab Director-- -� - <br />