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110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> F4I b=://wwwmccaml2bell.co E-mail main@mccampbell com <br />'•' Date Sampled 06/15/98 <br /> Advanced GeoEnvironmental Client Protect ID #0128,Arco <br /> 4005 North Wilson Way <br /> Date Received 06/17/98 <br />' Stockton,CA 95205 Client Contact Bill Little Date Extracted 06/20/98 <br /> Client P Q Date Analyzed 06/20/98 <br />' Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 90590 <br />' Client ID MW6/6-15-98 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND<230 Ethylbenzene 2000 <br /> Benzene 890 Hexachlorobutadiene ND<100 <br /> Bromobenzene NIX100 lodomethane ND<100 <br /> Bromochloromethane ND<100 Isopropylbenzene ND<100 <br /> I Bromodichloromethane NLK100 p-lsopropyl toluene ND<100 <br /> Bromoforrrt ND<100 Methyl butyl ketone N13<100 <br /> Bromomethane N13<100 Methylene Chloride") N13<100 <br /> n-Butyl benzene ND<100 Methyl ethyl ketone ND<100 <br /> sec-Butyl benzene NI3<100 Methyl tsobutyl ketone" ND<100 <br /> tert-Butyi benzene ND<100 Methyl tert-Butyl Ether(MTBE) <br /> Carbon Disulfide ND<100 Naphthalene ND<560 <br /> Carbon Tetrachloride ND<100 n-Propyl benzene ND<100 <br /> Chlorobenzene N13<100 Styrene ND<100 <br /> Chloroethane ND<100 1,1,1,2-Tetr2chloroethane ND<100 <br /> 2-Chioroethyl Vinyl Ethe ND<100 1,42,2-Tetrachloroethane ND<100 <br /> Chloroform ND<100 Tetrachloroethene N13<100 <br /> Chloromethane ND<100 Toluene 140 <br /> 2-Chlorotoluene ND<100 1,2,3-Tnchlorobenzene ND<100 <br /> 4-Chlorotoluene ND<100 1,2,4-Tnchlorobenzene N D<I 00 <br /> Dibromochloromethane ND<100 1,1,1-Tnchloroethane ND<100 <br /> 1,2-Dibromo-3-chloropropane ND<100 1,1,2-Tnchloroethane ND<100 <br /> Dibromornethane ND<100 Trichloroethene ND<100 <br /> 1,2-Dichlorobenzene N13<100 Trichlorofluoromethane ND<100 <br /> 1,3-Dichlorobenzene ND<100 1,2,3-Tnchloropropane ND<100 <br /> 1,4-Dichlorobenzene NDX100 1,2,4-Tnmethylbenzene 2300 <br /> Dichlorodifluoromethane ND<100 1,3,5-Tnmethylbenzene 680 <br /> 1,1-Dichloroethane ND<100 Vinyl Acetate ND<100 <br /> 1,2-Dichloroethane ND<100 Vinyl Chloride"' ND<100 <br /> 1,1-Dichloroethene NDa100 Xylenes,total '° 6800 <br /> cis-1,2-Dichioroethene ND<100 <br /> trans-l,2-Dichloroethene ND<100 <br /> 1,2-Dichloroprop2ne ND<100 <br /> 1,3-Dichloropropane ND<100 <br /> 2,2-Dichloropropane ND<100 Comments <br /> l,]-Dichloropropene ND<100 Surrogate Recoveries(%) <br /> cis-1,3-Dichloropropene ND<100 Dibromofluoromethane 111 <br /> trans-l,3-Dichloropropene ND<100 Toluene-d8 102 <br /> Ethylene dibromide ND<100 4-Bromofluorobenzene 98 <br /> .water and vapor samples are reported to ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 10 ug/L, vapor samples 05 ug/L, solid and sludge samples 5 ug/kg, wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit,N/A means analyte not applicable to this analysts <br /> (b) 2-propanone ar dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol % <br /> sediment,0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,(1)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethane, m <br /> (o)dimethylbenzenes ' <br /> DHS Certification No 1644 /1 Edward Hamilton,Lab Director <br />