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' 110 2nd Avenue South #D7 Pacheco,CA 94553 5560 <br /> McCaril�bell Analytical IncTelephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccampbell corn E-mail mainQmccampbell com <br /> ' Shaw Environmental&Infrastrue Client Project ID #779950 Date Sampled 05/16/02 <br /> 4005 Port Chicago Hwy Date Received 05/17/02 <br /> ' Concord, CA 94520 Client Contact Shelby Lathrop Date Extracted 05/17/02 <br /> Client P O Date Analyzed 05/17/02 <br /> ' Volatiles Organics by GC/MS(Basic Target List) <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order-0205253 <br />' Lab ID 0205253-003A <br /> Client ID AIR SPV-2 <br /> Matrix Air <br /> ` g <br /> Compound Concentration * DF Lt Compound Concentration * DF Repoli. <br /> L°�mtit <br /> Acetone ND<25 50 5 tert-Amyl methyl ether(TAME) ND<2 5 50 05 <br /> Benzene ND<2 5 so 0 5 Bromobenzene ND<2 5 50 0 5 <br /> Bromochloromethane ND<2 5 50 0 5 Bromodichloromethane ND<2 5 50 0 5 <br />' Bromoform ND<2 5 50 0 5 Bromomethane ND<2 5 50 0 5 <br /> 2-Butanone(MEK) ND<5 0 50 1 t-Butyl alcohol(TBA) ND<25 50 5 <br /> n-Butyl benzene ND<2 5 5 0 0 5 sec-Butyl benzene ND<2 5 5 0 0 5 <br /> tert-Butyl benzene ND<2 5 60 05 Carbon Ihsulfide ND<2 5 50 0 5 <br />' Carbon Tetrachloride NIX2 5 5 0 05 Chlorobenzene ND<2 5 50 0 5 <br /> Chloroethane ND<2 5 50 0 5 2-Chlomethyl Vinyl Ether N1[<5 0 50 1 <br /> Chloroform ND<2 5 5 0 05 Chloromethane ND<2 5 so 0 5 <br />' 2-Chlorotoluene ND<2 5 5 0 05 4-Chlorotoluene ND<2 5 50 0 5 <br /> DibromochloTomethane ND<2 5 5 0 0 5 1,2-Dibromo-3-chloropropane ND<5 0 50 1 <br /> 1,2-Dibromoethane(EDB) ND<2 5 5 0 0 5 Dibromomethane ND<2 5 50 05 <br /> 1,2-Dichlorobenzene ND<2 5 50 0 5 1,3-Dichlorobenzene ND<2 5 5 0 0 5 <br /> 1,4-Dichlorobenzene ND<2 5 5 0 0 5 Dichlorodifluoromethane ND<2 5 50 0 5 <br /> 1,1-Dichloroethane ND<2 5 50 0 5 1,2-Dichloroethane(I 2-DCA) ND<2 5 50 0 5 <br /> I,I-Dichloroethene ND<2 5 50 05 cis-1,2-Dichloroethene ND<2 5 50 0 5 <br /> trans-1,2-Dichloroethene ND<2 5 5 0 05 1,2-Dichloropropane ND<2 5 50 05 <br />' 1,3-Dtchloropropane ND<2 5 50 05 2,2-Dichloropropane ND<2 5 50 0 5 <br /> IJ-Dichloropropene ND<2 5 5 0 05 cis-1,3-Dichloropropene ND<2 5 50 0 5 <br /> trans-1,3-Dichloropropene ND<2 5 5 0 05 Dnsopropyl ether(DIPE) ND<2 5 5 0 05 <br /> Ethyl benzene ND<2 5 5 0 05 Ethyl tert-butyl ether(ETBE) ND<2 5 50 0 5 <br />' Hexachlorobutadiene ND<25 5 0 5 2-Hexanone ND<2 5 50 0 5 <br /> Iodomethane(Methyl iodide) ND<2 5 5 0 0 5 Isopropylbenzene ND<2 5 5 0 0 5 <br /> 4-Isopropyl toluene ND<2 5 5 0 0 5 Methyl-t-butyl ether(MTBE) 110 50 0 5 <br /> Methylene chloride ND<6 0 50 0 5 4-Methyl-2-pentanone(MIBK) ND<2 5 50 0 5 <br />' Naphthalene ND<25 5 0 5 Styrene ND<2 5 50 0 5 <br /> 1,1,1,2-Tetrachloroethane ND<2 5 5 0 05 1,1,2,2-Tetrachloroethane ND<2 5 50 0 5 <br /> Tetrachloroethene ND<2 5 50 1 05 Toluene ND<2 5 50 0 5 <br /> 1,2,3-Tnchlorobenzene ND<2 5 5 0 05 1,2,4-Trichlorobenzene ND<2 5 50 0 5 <br /> 1,1,1-Trichloroethane ND<2 5 5 0 0 5 1,1,2-Trichloroethane ND<2 5 50 0 5 <br /> Trichloroethene ND<2 5 5 0 05 Trichlorofluoromethane ND<2 5 50 0 5 <br /> 1,2,3-Trichloropropane ND<2 5 5 0 05 1,2,4-Tnrnethylbenzene ND<2 5 50 0 5 <br /> 1,3,5-Tnmethylbenzene ND<2 5 5 0 0 5 Vinyl Acetate ND<25 50 5 <br />' <br /> Vinyl Chloride ND<2 5 5 Q 0 5 Xylenes NIX2 5 50 0 5 <br /> Surrogate Recoveries(%) <br /> %SS 1 112 %SS2 J98 4 <br />' %553 987 <br /> Comments <br /> **Water and vapor samples are reported in ug/L,soil and sludge samples to ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts to ug/L <br />' ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> (h)lighter than water immiscible sheen/product is present,(i)liquid sample that contains greater than—2 vol %sediment,0)sample diluted due to <br /> high organic content <br />' DHS Certification No 1644 Edward Hamilton,Lab Director <br />