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' 110 2nd Avenue South kD7 Pacheco CA 94553-5560 McCarrlpbell Analytical Inc Telephone 925-798-1620 Fax 925-798-1622 hap/lwww mccampbell corn E-mail main@mccampbell com ' Shaw Environmental&Infrastruc Client Project 1D #779950 Date Sampled 05/16/02 4005 Port Chicago Hwy Date Received 05/17/02 ' Concord, CA 94520 Client Contact Shelby Lathrop Date Extracted 05/17/02 Client P O Date Analyzed 05/17/02 ' Volatiles Organics by GUMS(Basic Target List) Extraction Method SW503013 Analytical Method SW8260B Work Order 0205253 ' Lab ID 0205253-005A Client ID AIR SPV-I Matrix Air Compound Concentration * DF eUZ Compound Concentration * DF `i°°m ng Acetone ND<25 50 5 tert-Amyl methyl ether(TAME) ND<2 5 50 05 Benzene 93 50 0 5 Bromobenzene ND<2 5 5 0 0 5 Bromochloromethane ND<2 5 50 0 5 Bromodichloromethane ND<2 5 50 0 5 Bromoform ND<2 5 5 0 0 5 Bromomethane ND<2 5 50 0 5 2-Butanone(MEK) ND<5 0 5 0 1 t-Butyl alcohol(TBA) ND<25 5 0 5 n-Butyl benzene ND<2 5 5 0 0 5 sec-Butyl benzene ND<2 5 5 0 05 tert-Butyl benzene ND<2 5 5 0 0 5 Carbon Disulfide ND<2 5 5 0 05 ' Carbon Tetrachloride ND<2 5 5 0 0 5 Chlorobenzene ND<2 5 5 0 0 5 Chloroethane ND<2 5 5 0 0 5 2-Chloroethyl Vinyl Ether ND<5 0 5 0 1 Chloroform ND<2 5 5 0 0 5 Chloromethane ND<2 5 5 0 0 5 2-Chlarotoluene ND<2 5 5 0 0 5 4-Chlorotoluene ND<2 5 50 05 Dibromochloromethane ND<2 5 5 0 0 5 1,2-Dibromo-3-chloropropane ND<5 0 5 0 1 1,2-Dibromoethane(EDB) ND<2 5 5 0 1 05 Dibromomethane ND<2 5 50 0 5 1,2-Dichlorobenzene NIX2 5 50 1 0 5 1,3-Dichlorobenzene ND<2 5 5 0 0 5 1,4-1)ichlorobenzene ND<2 5 50 05 Dichlorodifluoromethane ND<2 5 50 05 ],I-Dichloroethane ND<2 5 50 0 5 1 2-Dichloroethane(1,2-DCA) ND<2 5 5 0 0 5 I,I-Diebloroethene ND<2 5 50 0 5 cis-1,2-Dichloroethene ND<2 5 so 05 trans-1,2-Dichloroethene ND<2 5 5 0 0 5 1,2-Dichloroprop2ne ND<2 5 50 0 5 I,3-Dichloropropane ND<2 5 50 0 5 2,2-Dichloropropane ND<2 5 50 05 l,l-Dichloropropene ND<2 5 5 0 1 0 5 cis-1,3-Dichloropropene ND<2 5 5 0 0 5 trans-l,3-Dichloropropene ND<2 5 5 0 1 05 Dnsopropyl ether(DIPS) ND<2 5 50 0 5 Ethyl benzene 37 50 0 5 Ethyl tert-butyl ether(ETBE) ND<2 5 50 05 ' Hexachlorobutadiene ND<25 5 0 5 2-Hexanone ND<2 5 50 0 5 Iodomethane(Methyl iodide) ND<2 5 50 0 5 Isopropylbenzene 2 8 5 0 0 5 4-Isopropyl toluene ND<2 5 5 0 0 5 Methyl-t-butyl ether(MTBE) 69 50 0 5 Methylene chloride ND<6 0 5 0 0 5 4-Methyl-2-pentanone(MIBK) NDQ 5 5 0 0 5 Naphthalene ND<25 5 0 5 Styrene ND<2 5 50 05 1,1,1,2-Tetrachloroethane ND<2 5 5 0 0 5 1,1,2,2-Tetrachloroethane ND<2 5 50 05 Tetrachloroethene ND<2 5 50 05 Toluene 84 50 1 05 1,2,3-Trichlorobenzene ND<2 5 50 05 1,2,4-Tnchlorobenzene ND<2 5 50 0.5 ' 1,1,1-Tnchloroethane ND<2 5 50 05 1,1,2-Tnchloroethane ND<2 5 50 05 Trichloroethene ND<2 5 so 05 Trichlorofluoromethane ND<2 5 50 05 1,2,3-Tnchloropropane ND<2 5 50 05 1,2,4-Tnmethylbenzene 41 50 --05 1,3,5-Trlmethylbenzene 20 50 05 Vinyl Acetate ND<25 50 5 ' Vin 1 Chloride ND<2 5 1 5 0 0 5 Xylenes 190 1 50 05 Surrogate Recoveries(%) %SS 1 113 %SS2 968 %S53 ]0] Comments "water and vapor samples are reported in ug/L.,sod and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis . (h)lighter than water immiscible sheen/product is present,(1)liquid sample that contains greater than—2 vol %sediment,(1)sample diluted due to high organic content DHS Certification No 1644 �1,tM�Edward Hamilton,Lab Director