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LAB CORE LABORATORIES S U R R O G A T E R E C O V E R I E S R E P O R T Job Number - 991748 Report Date 09/09/1999 CUSTOMER. IT Group PROJECT: Southland - Martinez ATTN. Bob Butter Method Volatile Organics by GC/MS Batch 8274 Method Code 82600X Analyst gfb Surrogate Vnits Dibromofluoromethane ug/L Lab ID Matrix QC Type Dilution Result True Value Percent Recovery Limits Flag Date Time LCS 1 22 85 25 000 91 4 57-162 09/01/1999 1013 MB 1 22 06 25 000 88 2 57-162 09/01/1999 1041 991744-2 Liquids 20 23 42 25 000 93 7 57-162 09/01/1999 1139 991673-1 Liquids 1 23 38 25 000 93 5 57-162 09/01/1999 1208 991745-7 Liquids 1 22 44 25 000 89 8 57-162 09/01/1999 1236 991745-8 Liquids 1 22 65 25 000 90 6 57-162 09/01/1999 1305 991745-9 Liquids 1 20 98 25 000 83 9 57-162 09/01/1999 1334 991747-1 Liquids 1 21 31 25 000 85 2 57-162 09/01/1999 1402 991747-3 Liquids 1 22 81 25 000 91 2 57-162 09/01/1999 1500 991747-5 Liquids 1 23 11 25 000 92 4 57-162 09/01/1999 1528 07 45-6 Liquids 1 23.74 25 000 95 0 57-162 09/01/1999 1557 45-6 Liquids MS 24 08 25 000 96 3 57-162 09/01/1999 1626 45-6 Liquids MSD 25 16 25 000 100 6 57-162 09/01/1999 1655 991745-2 Liquids 4 24 55 25 000 98.2 57-162 09/01/1999 1723 1991745,5 Liquids 40 23 11 25 000 92 4 57-162 09/01/1999 1752 991748-2 Liquids 1 23 04 25 000 92 2 57-162 09/01/1999 1849 991748-3 Liquids 1 22 42 25 000 89 7 57-162 09/01/1999 1918 991748-5 Liquids 1 21 74 25 000 87 0 57-162 09/01/1999 2016 991747-2 Liquids 40 22 23 25 000 88 9 57-162 09/01/1999 2045 Method Volatile Organics by GC/MS Batch 8318 Method Code 82600X Analyst gfb Surr(4ate Units Dibromofluoromethane ug/L Lab ID Matrix QC Type Dilution Result True Value Percent Recovery Limits Flag Date Time LCS 1 28.06 25 000 112 2 57-162 09/02/1999 1617 MB 1 25.82 25 000 103.3 57-162 09/02/1999 1645 991748-1 Liquids 20 26 78 25 000 107 1 57-162 09/02/1999 1714 991749-3 Liquids 1 27 82 25 000 111 3 57-162 09/02/1999 1811 991758-1 Liquids 1 25.70 25 000 102 8 57-162 09/02/1999 1840 991758-2 Liquids 1 27.20 25 000 108 8 57-162 09/02/1999 1909 991758-3 Liquids 1 26 94 25 000 107 8 57-162 09/02/1999 1937 991758-4 Liquids 1 26 97 25 000 107 9 57-162 09/02/1999 2006 991758-6 Liquids 100 22 49 25 000 90 0 57-162 09/02/1999 2104 991758-1 Liquids MS 22 97 25 000 91.9 57-162 09/02/1999 2133 941758-1 Liquids MSD 23 51 25 000 94 0 57-162 09/02/1999 2202 991748-4 Liquids 50 25 00 25 000 100 0 57-162 09/02/1999 2230 059-1 Liquids 1 24.67 25 000 98 7 57-162 09/02/1999 2328 59-4 Liquids 1 24 81 25 000 99 2 57-162 09/03/1999 0055 1 Page 14 rna enelNca!rasuns ap mans or iMerprelalana oontalned n Ihs rapan eta pesetl upon Inlorrnelgn antl malarial aWoi by Ina 01 IW whom—Ii,swe and cont 0eneel use INS repot nes baen made The irwlYtical—L to Upexon5 W nlIXf]rala[ions iameseea rapresanl the oast lud(Iment o!Core Labondones Care Laboralones makes rw-ar arty a reprasantetpn aapnss of Nni OI my type and a.0,i d Si uT-as!o INS prodpcimty proper opariUoni M ptaetabei o! .f o1 pas Ops!IX Olney__I prq_,y sap,,d sand in—ii.nln whch each r.OW 4 peal ar r"ad ppan i any rasion amalspeen The nfpon alrtl!rcpt-ratradpLad In wbde d in par•mti Me Wuhan apprWN of Core Laboramrles