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1 ' S U R R O G A T E R E C O V E R I E S R E P O R T Job Number 200279 Report Date. 02/18/2000 ' CUSTOMER IT Group PROJECT; Southland - Martinez ATTN Rhonda Teicheira ' Method Volatile Organics -Aromatics Batch 10999 Method Code 8020BX Analyst evd ' Surrogate Units 4-Bromofluorobenzene ug/L ' Lab ID Matrix OC Type Dilution Result True Value Percent Recovery Limits flag Date Time MB 1 47 24 50 0000 94 5 64-147 02/09/2000 1042 LCS 1 48 77 50.0000 97 5 64-147 02/09/2000 1246 LCD 1 48 45 50.0000 96 9 64-147 02/09/2000 1312 200278-3 Liquids 1 35 90 50 0000 71 8 64-147 02/09/2000 1337 200279-5 Liquids 1 36 67 50 0000 73.3 64-147 02/09/2000 1403 200280-3 Liquids 1 36 33 50 0000 72 7 64-147 02/09/2000 1429 200280-2 Liquids 25 45 03 50 0000 90 1 64-147 02/09/2000 1454 200281-1 Liquids 5 40 15 50 0000 80 3 64-147 02/09/2000 1546 200279-3 Liquids 10 38.92 50 0000 77 8 64-147 02/09/2000 1611 200279-4 Liquids 100 36.00 50 0000 72.0 64-147 02/09/2000 1637 200278-2 Liquids 5 37.07 50 0000 74 1 64-147 02/09/2000 1703 W277-3 Liquids 10 34 67 50 0000 69 3 64-147 02/09/2000 1936 277-2 Liquids 10 36 72 50 0000 73 4 64-147 02/09/2000 2002 280-1 Liquids 25 34 27 50 0000 68 5 64-147 02/09/2000 2327 200299-4 Liquids MS 1 33 556 50 0000 67 1 64-147 02/11/2000 0049 200299-4 Liquids MSD 1 32 52 50 0000 65 0 64-147 02/11/2000 0115 Method Volatile Organics by GC/MS Batch 11004 Method Code 8260OX Analyst .. gfb 1 Surrogate Units ' Dibromofluoromethane ug/L Lab ID Matrix OC Type Dilution Result True Value Percent Recovery Limits Flag Date Time ' 200240-2 Liquids 1 25.99 25 000 104 0 57-162 02/01/2000 1627 200240-2 Liquids MS 26.26 25 000 105 0 57-162 02/01/2000 2013 200240-2 Liquids MSD 25 40 25 000 101 6 57-162 02/01/2000 2041 200262-21 Solid 1 23 33 25 000 93.3 60-160 02/04/2000 0502 ' 200262-21 Solid MS 23.52 25.000 - 94 1 60-160 02/04/2000 0914 200262-21 So€id MSD 23.28 25 000 93 1 60-160 02/04/2000 0945 200271-9 Liquids 2000 22 00 25 000 88 0 57-162 02/09/2000 0128 LCS 1 22 51 25 000 90 0 57-162 02/09/2000 0201 200271-10 Liquids 1000 22 62 25 000 90 5 57-162 02/09/2000 0236 ' 200277-2 Liquids 20 22 36 25 000 89 4 57-162 02/09/2000 0307 200280-1 Liquids 50 21.47 25 000 85 9 57-162 02/09/2000 0339 200280-2 Liquids 100 22.10 25 000 - 88 4 57-162 02/09/2000 0410 200280-3 Liquids 1 21 91 25 000 87 6 57-162 02/09/2000 0441 200281-1 Liquids 1 21 56 25 000 86 2 57-162 02/09/2000 0512 ' 200278-1 Liquids 1 21 75 25 000 87 0 57-162 02/09/2000 0545 200278-2 Liquids 2 22 27 25 000 89 1 57-162 02/09/2000 0616 W2 278-3 Liquids 1 21 79 25 000 87 2 57-162 02/09/2000 0648 78-4 Liquids 1 22 02 25 000 88 1 57-162 02/09/2000 0719 ' 79-1 Liquids 1 22 63 25 000 90 5 57-162 02/09/2000 0750 Page 17