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1 <br /> CofiLAB CORE LABORATORIES <br /> Q U A L I T Y C 0 N T R 0 L R E S U L T S <br /> Job Number 981252 Date 09/09/98 <br /> CUSTOMER fluor Daniel GTI PROJECT 102455-6304 ATTN Shelby Lathrop <br /> QC Type Description Reag Code Lab ID Dilution Factor Date Time <br /> M8 Method Blank 08/28/98 1006 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits <br /> Benzene 0 0 5000 <br /> Ethylbenzene 0 n.5000 <br /> Methyl-t-Butyi Ether (MTBE) 2 007 10 0000 <br /> oluene 0 182 0 5000 <br /> ylenes (total) 0 00 0 5000 <br /> OVContinuing Calibration Verification 08030501A 08/28/98 0533 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits <br /> Benzene 21 032 20 105 D 85-115 <br /> Ithylbenzene 18 449 20 92 D 85-115 <br /> ethyl-t-Butyl Ether (MTBE) 26 887 20 134 0 70-130 <br /> oLuene 19 936 20 100 D 85-115 <br /> Xylenes (total) 57 70 60 96 D 85-115 <br /> S Matrix Spike 08030501A 981253-8 08/28/98 0905 <br /> Parameter/Test Description QC Result QC Result True Value 0rig Value Caic Result * Limits <br /> enzene 21 603 20 0 108 0 % 39-150 <br /> thylbenzene 19 007 20 0 95 0 % 32-160 <br /> Methyl-t-Butyl Ether (MTBE) 32 904 20 2 559 151 7 % 50-150 <br /> oluene 20 001 20 0 160 99 2 % 46-148 <br /> ylenes (total) 60 19 60 0 00 100 3 % 75-125 <br /> MSD Matrix Spike Duplicate G8030501A 981253-8 08/28/98 fl935 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits <br /> Benzene 22 552 21 603 20 0 112 8 % 39-150 <br /> 4 R 20 <br /> thylbenzene 19 454 19 007 20 0 97 3 % 32-160 <br /> 2 R 20 <br /> Methyl-t-Butyl Ether (MTBE) 33 250 32 904 20 2 559 153 5 % 50-150 <br /> 1 R 25 <br /> oluene 20 643 20 001 20 0 160 102 4 % 46-148 <br /> 3 R 20 <br /> kylenes (total) 61 26 60 19 60 0 00 102 1 % 75-125 <br /> 2 R 20 <br /> CV Continuing Calibration Verification 08030501A 08/29/98 0136 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits <br /> Uenzeberizene <br /> ne 22 348 20 112 D 85-115 <br /> 19 242 20 96 D 85-115 <br /> t-t-Butyl Ether (MTBE) 29 684 20 148 D 70-130 <br /> .*Tn20 328 20 102 D 85-115 <br /> Page 6 <br /> REC R-RPD A-ABS Diff D-% Diff <br /> I t o IyIT 9 qs o[t n 3 of rt np t t O s cont btl r 11 s oo t d [a5 !wxID 1 o nater i ppl W by Me cl onl 1P.nose a cl s e and conitlxnl tl v to s 01 nos O� mIle rN amyl Ca as I45 ult ons o me p e1d I ons <br /> 1 n r n ` ec t In t I I IaPy o!u Gn Woo 3to a Gpe L bo tlo xns �V„ne t 4nso3o'a only�xi I w t vl On son xss o 9 ttwt Pt a Y t llx ntl n t a54iy o scfaP s Smm�is looan n cYlo ctiv x n Ooe o0o sI W W P of t aulenn5s al <br /> I s P Ptl no a Ifba t qn 5a V cPnnq^I en w It w oo I 5r 0 al stl Ita150 �f,5 e00 t Shay nol ba P otl�cwl wnpin t1 x t tr n w Hp oval of Co n L VO—1 es <br />