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1 COULAB CORE LABORATORIES S U R R O G A T E R E C O V E R i E S R E POR T Job Number 981252 Report Date 09/09/98 CUSTOMER Fluor Daniel GTI PROJECT 102455-6304 ATTN. Shelby Lathrop Method EPA 8020A Batch 2656 Method Code 8020BX Analyst sdg Surrogate Units 4-Sromofluorobenzeneug/L Lab ED Matrix _QC Type Dilution Result True Value Percent Recovery Limits Flag Date Time IV 1 101 798 100 000 101 8 64-147 08/28/98 0936 Me 1 90 924 100 000 90 9 64-147 08/28/98 1006 81250-1 Liquids 500 106 634 100 000 106 6 64-147 08/28/98 1159 81250-2 Liquids 500 103 113 100 000 103 1 64-147 08/28/98 1229 81250-3 Liquids 500 98 449 100 000 98 4 64-147 08/28/98 0100 981250-4 Liquids 500 107 916 100 000 107 9 64-147 08/28/98 0130 981250-5 Liquids 100 101 772 100 000 101 8 64-147 08/28/98 0200 181252-1 Liquids 1 94 228 100 000 94 2 64-147 08/28/98 0231 81260-1 Solid 1 89 955 100 000 90 0 64-147 08/28/98 0301 81252-3 Liquids 1 105 127 100 000 105 1 64-147 08/28/98 0332 981253-3 Liquids 1 121 311 100 000 121 3 64-147 08/28/98 0402 20 1 102 415 100 000 102 4 64-147 08/28/98 0432 CV 1 93 269 100 000 93 3 64-147 08/28/98 0533 53-5 Liquids 1 101 686 100 000 101 7 64-147 08/28/98 0604 P811253-6 Liquids 1 95 798 100 000 95 8 64-147 08/28/98 0634 981253-7 Liquids 1 101 323 100 000 101 3 64-147 08/28/98 0704 181253-8 Solid 1 100 758 100 000 100 8 64-147 08/28/98 0734 81253-8 Solid MS 107 555 100 000 107 6 64-147 08/28/98 0905 81253-8 Solid MSD 110 965 100 000 111 0 64-147 08/28/98 0935 981253-9 Solid 1 94 617 100 000 94 6 64-147 08/28/98 1005 081253-10 Solid 1 95 078 100 000 95 1 64-147 08/28/98 1036 81253-1 Liquids 1 122 056 100 000 122 1 64-147 08/28/98 1106 81253-2 Liquids 10 102 056 100 000 102 1 64-147 08/28/98 1136 81258-1 Liquids 1 97 335 100 000 97 3 64-147 08/29/98 0006 981258-2 Liquids 1 93 019 100 000 93 0 64-147 08/29/98 0036 CV 1 97 173 100 000 97 2 64-147 08/29/98 0136 81258-3 Liquids 1 105 292 100 000 105 3 64-147 08/29/98 0207 181252-2 Liquids 1 100 282 100 000 100 3 64-147 08/29/98 0237 981253-4 Liquids 1 112 072 100 000 112 1 64-147 08/29/98 0307 CV 1 103 699 100 000 103 7 64-147 08/29/98 0407 Method EPA 82608 Batch 2779 Method Code 8260OX Analyst daf Surrogate Units Dibromofluoromethane ug/L Lab ID Matrix QC Type Dilution Result True Value Percent Recovery Limits Flag Date Time MB 25 73 25 000 102 9 79-132 09/04/98 1659 81252-1 Liquids 1 26 37 25 000 105 5 79-132 09/04/98 1737 1;*2-2 Liquids 1 25 85 25 000 103 4 79-132 09/04/98 1815 -3 Liquids 25 25 52 25 000 102 1 79-132 09/04/98 1853 -1 Liquids 1 26 42 25 000 105 7 79-132 09/04/98 1932 Page 9 rn..analylmar es,rns oo an y o my i rarm o s cwel ten n n s rnw r r y oa do I Ixnt nru m r nn,.a:,r I I s nul nil vv na n m{rn wnnse o crus x ann ro I n m v{use ms sae.{nos r>�t maga rM1a ane yl c tl assns Dan o s w mo o eta I o s e Y a yw1 cnAs o{Inn oesl II J 1 nn r nl Gorn LahoaMl�n�o I.—t mora o 5 f wyrr soon re no w r rn rr u el f l I r e n ysv or ImN nd of anY IYIw r xl n o H�sly o S�la^ws Deeps[o Ins Ornct IV o enx oVa a of s o ar91{a bre oss 0 l a s n1r e n[r ty w!1 0 �r cn �I a'd o rel a l ufwn la i wr {y�xuy M1 s y o l sna 1 not try y pa I .[nOtrl Ir y w l e t app O s o CdB L.Dda e5