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MINIMUM VERIFICATION LABORATORY ANYSIS" <br /> PCO <br /> TANK TANK � ITII-tl TPIi-D BTX & E CL iiC TOTAL EDD METCAPD 8270 <br /> 8010 LEAD <br /> CON"IENTS 80115 15 8020 8265 8 6(1 8220 8240 7420 8240 AES or 8080 <br /> 7421 AA <br /> ,41 LEADED X X X <br /> �� <br /> OAS X <br /> UNL OAS X X <br /> 4896', DiPSEL X ---..X— ----- ------ <br /> KEROSENE X X <br /> . --- x X X X <br /> UNK FUEL X — ------ <br /> �– _ x <br /> 01L X <br /> CIILOR• X X <br /> SOLVENTS ----- <br /> NONCI iLOR X <br /> SOLVENTS �—_ ----- <br /> WASM X X X <br /> USED 011, x x <br /> ethods <br /> In <br /> All analyses m <br /> ethods ate designated EPA methods described In EPA SW 84d,Thi�d Edpl Jix T Table 3-5 forldetection <br /> SW 846,arc specifically noted,below. Refer to the "SWItCB LUFl"Field Manual ,Appendix <br /> Ilmlts of tnr?tot vehicle fuels•{gnsolloe and dlesel). Reref to 1-2-3 'Regional <br /> ion card Staff Recommendations for Initial <br /> Evaluation and investigation of US I s for the waste and <br /> motor iletectfon I,Imlta lhot remain below the MCI., 5311,0 orinble Limit of the contnrrtinnnl In S�testion will be accepted, <br /> hosterer laboratory #hell utilize Me most cottser,ative method. <br /> 1.A00RA'fbRY ANALYSf:S 'IERMINOI.(7OY: 001-111) (5113(1} 8015 mod yr OC/MS 8260 <br /> TPII-U Total Petroleum Ilydrocatbon, Uasollne, <br /> TPII-i) 7o1a1 Petroleum Ilydrocarbon, Diesel, OC/f'ID (3550), 8515 mod'or'OCIMS 8260 <br /> II'i'X A E Benzene, Toluene, Xylene & Ethyl Benzene, OC/PiI) 8025 or (IC/MS 8260 <br /> CL IiC Chlorinated Ilydrocatbon, OC ISD Solo, OC/MS 8240 <br /> Total Lead Total (end, AA 7420, AA 7421 nr ICP-Ar1S 6010 <br /> Ethylene dibromide (131 MAD 1803), ODMS 8240 (DI IS-Luft) <br /> I=U© <br /> C1C FiD Oas Chromatography, blame Ionization Detection <br /> ICAP of AA Inductively Ch Coupled Plasma Atomic Emission Spectrometry 6510 or 'Atomic Absorption <br /> spectrometry 7(xlo. Metals: Cadmium, Chromium III and Vi, Lend, and Zinc. •+1'4k� <br /> PCH Palychlorinaled Blphenyis, OC/MS 8275 or 8580 <br /> Method 3050 Act([ digestion <br /> Melhnd 3540 Soxhlet sample pteparatlan <br /> Melhod 3550 Sonication sample preparation, extraction method <br /> Method 5030 Purge and Trap sample preparation <br /> QA/QC Quality Assufance/Quality Control <br /> ary columns ate <br /> Notes: To avoid false positive detection of benzene, ebe scd asra eri stv utswith Fire i dlttyo be*samples oronceltthe hydrocarbons <br /> preferred to packed columns, a packed column may <br /> have been characterized and proper QA/AC Is followed. <br /> For )[Inking walet svutces, EPA recommentis that (he 505 series for volatile organics be used In preference to the 600 scrics <br /> because the detection limits are lower (lie QA/QC Is better. <br /> Ell 23 048 (Rev 1 Page 8 <br />