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110 2nd Avenue South,##D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />' http://www.mgcampbell co m E-mail mato@mccampbell com <br /> Advanced GeoEnvironmental Client Protect ID Tracy Marine Sales <br /> Date Sampled 11/08-11110199 <br /> 4005 North Wilson Way Date Received 11/12/99 <br /> Stockton,CA 95205 Client Contact Bill Little Date Extracted 11/12-11/15/99 <br /> Client P O Date Analyzed 11/12-11/15/99 <br /> Gasoline Range(C6-02)Volatile Hydrocarbons as Gasohne*,with Methyl tert-Butyl Ether* &BTEX* <br /> EPA methods 5030,modified 8015,and 8020 or 602,California RWQCB(SF Bay Region)method GCFID(5030) <br /> ILab ID Client ID MamEthylben- %Recovery x TPH(g)+ MTBE Benzene Toluene Zene Xylenes Surrogate <br /> 25443 MW1-5 S NO NO NO ND NO NO 103 <br /> 25444 MW1-10 S NO ND ND NO NO NO 102 <br /> 25445 MW2-10 S 2 ],a ND<0 10 0 012 0 068 0 057 022 ---" <br />' 25446 MW2-15 S NO NO 00060 0 029 0 013 0 061 100 <br />' 25447 MW2-20 S ND ND NO 00090 NO 0 016 103 <br /> 25448 MW3-10 S NO NTD ND NO NO NO 103 f^ <br /> 25449 MW3-15 S NO A'D NO NO NO NO 105 <br /> 25450 MW4-15 S NO NO NO 00070 NO 0 022 103 <br />' 25451 MW4-20 S NO NO NO NO NO 0 014 109 <br /> 25452 MW4-10 S NO NO 00060 0 023 0 016 0 072 103 <br />' 25453 MW4-5 S 69,b0 1 8 033 077 2 7 11 100 <br /> I25454 MW5-5 S 150,a 058 078 1 7 4 8 14 101 <br /> 25455 MW5-10 S 78,a ND<0 30 0 82 1 1 23 70 " <br />' 25456 MW5-15 S NO NO NO NO ND 0 017 102 <br /> Reporting Limit unless W 50 ug/L 50 05 05 05 05 <br />' otherwise stated,ND <br /> means not detected above S 1 0 mg/kg 005 0 005 0 005 0 005 0 005 <br /> the reporting limit <br /> *water and vapor samples are reported in uglL,wipe samples in ug/,Alpe,soil and sludge samples in mg/kg,and all TCLP and SPLP extracts <br />' in ug/L <br /> Cluttered chromatogram,sample peak coelutes with surrogate peak <br /> *The following descnptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not responsible for their <br />' interpretation a) unmodified or weakly modified gasoline is significant, b) heavier gasoline range compounds are significant(aged <br /> gasolme9), c) lighter gasoline range compounds (the most mobile fraction) are significant, d) gasoline range compounds having broad <br /> chromatographic peaks are significant biologically altered gasoline?,e)TAH pattern that does not appear to be derived from gasoline(1),0 <br /> one to a few isolated peaks present g)strongly aged gasoline or diesel range compounds are significant,h) lighter than mater immiscible <br />' sheen is present,i)liquid sample that contains greater than—5 vol %sediment,j)no recognizable pattern <br /> DHS Certification No 1644 A 1 Edward Hamilton, Lab Director <br /> I <br />