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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAWBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccamnbell.com E-mail main@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID Tracy Marine Sales Date Sampled 11/08-11/10/99 <br /> 4005 North Wilson Way Date Received 11/12/99 <br /> Stockton, CA 95205 Client Contact Bill Little Date Extracted 11/12/99 <br /> i <br /> Client P O Date Analyzed 11/12-11/16/99 <br /> Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab 1D 25454 25455 25456 25457 <br /> Reporting LimitClient ID MW5-5 MW5-10 MW5-15 MW6-26 <br /> Matrix S S S S S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(D1PE) ND<20 ND<13 ND ND 50 10 <br /> Ethyl tent-Butyl Ether(ETRE) ND<20 ND<13 ND ND 50 10 <br />' Methyl-cert Bury] Ether(MTBE) 430 210 ND 13 50 1 0 <br /> tert-Amyl Methyl Ether(TAME) ND<20 ND<13 ND ND 50 1 10 <br /> tent-Butanol ND<100 ND<65 ND ND 25 50 <br />' Surrogate Recoveries(%) <br />' Dibromofluoromethane 91 87 84 85 <br /> Comments <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP 1 STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than N%ater immiscible sheen is present, (i)liquid sample that contains greater than —5 vol IN,sediment 0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br /> I <br />