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i <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAM'BELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> Iht_tp//www me i bell com E-mail main@mccampbell com <br /> IAdvanced GeoEnvironnriental Client Project ID Three B's Date Sampled 09/06/01 <br /> 837 Shaw Road Date Received 09/07/01 <br /> Stockton,CA 95215 Client Contact Tim Cuellar Date Extracted 09112-09/14/01 <br /> I Client P O Date Analyzed 09/12-09/14/01 <br /> Seven Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 77224 77225 77226 77227 <br /> MW1/ MW2/ MW3/ MW4/ Reporting Limit <br /> Client ID 090601 090601 090601 090601 <br /> Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPS) ND<2 5 ND<2 5 ND<5 0 ND<5 0 50 10 <br /> IEthyl tent-Butyl Ether(ETBE) ND<2 5 ND<2 5 ND<5 0 ND<5 0 50 10 <br /> lieMethyl tert-Butyl Ether(MTBE) 47 ND<2 5 ND<5 0 110 50 1 0 <br /> tert-Amyl Methyl Ether(TAME) ND<2 5 ND<2 5 ND<5 0 ND<5 0 50 10 <br /> Itert-Butanol ND<12 5 ND<12 5 ND<25 ND<25 25 50 <br /> Methanol ND<1250 ND<1250 ND<2500 ND<2500 2500 500 <br /> IEthanol ND<125 ND<125 ND<250 ND<250 250 50 <br /> Surrogate Recoveries(%) <br /> IDibromofluoromethane 103 93 96 107 <br /> Comments <br /> I *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present (i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> Ihigh organic content <br /> I <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br /> I <br />