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1 <br /> McCampbell Analytical, Inc. 110 Telephonnd e <br /> 25-79South, 162 Pacheco,25 94553-5560 <br />' j I Tc] hone 925-798 1620 Fax 925 796 1522 <br /> Website www rnceamp6ell com E-mail mam(Er rnrcartipbell com <br /> iQC SUMMARY REPORT FOR SW801.5C <br />' W O Sample Matrix Water QC Matrix Water WorkOrder 0506512 <br />' EPA Method 8W8015C Extraction SW3510C BatchiD 16889 Spiked Sample ID NIA <br /> Analyte Sample Spiked _MS MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> jig/t. ug/L %Rea %Rec % RPD %Rea ' %Rec %RPD MS 1 MSD LCS!LCSD <br />' TPH(d) NIA 1000 NIA N/A I N/A 116 118 234 NIA 70- 130 <br /> %SS N/A 2500 NIA NIA NIA 1 105 102 298 NIA 70- 130 <br />' All target compounds in the Method Blank of this extraction hatch were ND less than the method RL with the following exceptions <br /> NONE <br /> BATCH 16889 SUMMARY <br />' Sample ID Date Sampled Date Extracted Date Analyzed Sample ID Date Sampled Date Extracted Date Analyzed <br /> 10506512-007B 6127105 9 46 AM 6/28105 6/29/05 7 01 PM 0506512-008B 6127105 10 31 AM 6!28/05 6/21/011 18 PM <br /> 0506512-0098 6127105 10 43 AM 6/28105 6/29105 8 06 AM 0506512-0108 6/27105 10 56 AM 6128/05 6129105 9 12 AM <br /> 06512-111 B 612710111 13 AM 6128105 6129105 10 35 AM 0506512-01211 6127/05 11 33 AM 6/28/01 6/29101106 AM <br />' 0--506512-013B 6/27/05 It 52 AM 6/28105 6/29/05 9 12 AM�_ <br /> I <br /> I <br /> MS=Matrix Spike MSD=Matrix Spike Duplicate LCS=Laboratory Control Sample LCSD=Laboratory Control Sample Duplicate,RPD=Relative Percent Deviation <br /> %Recovery=100"(MS-Sample)/(Amount Spiked) RPD=100`(MS- MSD)/((MS+MSD)12) <br /> MS/MSD spike recoveries and 1 or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample s matrix interferes with the spike recovery <br /> NIA=not enough sample to perform matrix spike and matrix spike duplicate <br /> NR=ana!Nte concentration in sample exceeds s ika amount for sold matrix or exceeds 2x spike amount for water matrix or sem le diluted due to high matrix or anal&e content <br /> IR <br /> HS Certification No 1644 �QAIQC Officer <br /> I <br />