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Ave <br /> 51 <br /> McCampbell Analytical, Inc. ]i02le honeue25-798 1 7 Pacheco 25 98 1622 0 <br />' Telephone 925-74B 1620 Fax 925 798 1622 <br /> A4 1 Website www mccampbell com E mail mam(Lerm"mpbell com <br /> • QC SUMMARY REPORT FOR SW8021B/8015Cm <br />' W O sample Matrix Water QC Matrix Water WorkOrder 0506614 <br /> EPA Method SW8021B16015Cm Extractlon SW5030B BatchiD 16688 Spiked Sample ID 0506542-00SA <br />' Analyte Sample Spiked MS MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria{%) <br /> pg/L pC/L % Rec I %Rec %RPD %Rec % Rec %RPD MS/MS LCS 1 LCSD <br /> —71 <br />' TPH(btex)f ND 60 96 8 973 - 0 509 98 8 968 200 70- 130 70- 130 <br /> MTBE ND 10 103 102 0 532 975 934 429 70- 130 7D- 130 <br />' Benzine ND r30 <br /> 91 2 932 2 18 993 92 658 70- 130 70130 <br /> Toluene ND 92 3 942 202 101 903 109 70- 130 70-130 <br /> Ethylbenzene ND 947 963 _ 160 996 I 976 2 10 70- 130 70-130 <br />' Xylenes ND 957 993 376 100 100 0 70-130 70-130 <br /> °/a5S 104 10 95 97 2 29 103 99 3 97 70-130 70-130 <br />' All target compounds to the Method Blank of this extraction batch were ND less than the method RL with the following exceptions <br /> NONE <br /> BATCH 16888 SUMMARY <br />' am8 46 MP 05ple ID Date Sampled Date Extracted Date Analyzed Sample ID Date Sampled Date Extracted Date Analyzed <br /> 06514-OOIA 6/27105 9 26 AM 6129105 6129105 06514-002A 6127105 9 53 AM 6129/05 6/29/05 9 53 PM <br /> 0506514-003A 6/27105 10 22 AM 7101105 7/01/05 It 56 AM 0506514-004A 6/27105 10 37 AM 7/01/05 7101/05 12 30 PM <br />' D5065 1 4-00 5A 6127/05 10 55 AM 7101/05 71011/05 5 27 AM 0506514-1106A 6127105 11 13 AM 7101105 7101/01116 AM <br /> 0506514-007A 6,'27/05 1137 AM 7101/05 7/01105 6 26 AM 0506514-008A 6/27/05 l2 24 PM 7101/05 7!01/05 9 34 PM <br /> I <br /> 1 <br /> I <br />' MS=Matra Spike MSD=Matrix Spike Duplicate LCS=Laboratory Control Sample LCSD=Laboratory Control Sample Duplicate RPD=Relative Percent Deviation <br />' %Recovery=100'(MS-Sample)I(Amount Spiked) RPD=100'(MS- MSD)/((MS+MSD)12) <br /> MS/MSD spike recoveries and I or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked or b)the spiked sample's matrix interferes with the spike recovery <br />' £TPH(btex)=sum of B'TEX areas from the FID <br /> *N4cRL=anal <br /> matogram,sample peak coelutes with surrogate peak <br /> cable or not enough sample to perform matrix spike and matrix spike duplicate <br /> oncentration in sample exceeds spike amount for sail matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content <br /> DHS Certification No 1644 QA/QC Officer <br />