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1 <br /> CA 94553 <br /> 4 L McCampbell Analytical, Inc. 1 <br /> 10Te1 phone 92nd Avee 25 798#620�Faxn925 799 1622560 <br /> Website www mccampbell com E mail mam(ynx campbell corn <br /> 0 QC SUMMARY REPORT FOR SW8260B <br /> W 0 Sample Matrix Water QC Matrix Water WorkOrder 0506514 <br /> EPA Method SW82603 Extraetlon SW5130B BatchlD 16891 Spiked Sample ID 0506528-003A <br />' Analyte Sample Spiked - MS i MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> Ng/L Fig/L %Rec %Ree %RPD %Rec % Rec %RPI? MS I MSD LCS/LCSD <br /> tert-Amyl methyl ether(TAME) ND 10 992 975 174 101 101 0 70- 130 1 70-130 <br /> t-Butyl alcohol(TBA) ND 50 987 775 24 1 963 101 473 70- 130 70- 130 <br />' 1,2-Dibromoethane(EDB) ND LO - 96 998 380 957 958 0 149 70- 130 70- 130 <br /> 1,2-Dlchloroethane(1,2-DCA) ND 10 113 112 141 116 110 538 70-130 70-130 <br /> Dusopropyl ether(D1PE) ND 10 119 118 1 10 119 119 0 70-130 70 130 <br /> Ethyl tort-butyl ethel(ET13E) ND l0 103 997 356 111 103 777 70-130 70-130 <br /> Methyl-t-butyl ether(MTBE) ND 10 956 938 194 104 93 5 107 70-130 70-130 <br />' %SSI 105 10 92 84 379 95 89 7 10 70-130 70- 130 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions <br /> t NONE <br /> BATCH 16891 SUMMARY <br /> lample ID Date Sampled Elate Extracted Date Analyzed Sample 113 Date Sampled Date Extracted Date Analyzed <br /> 0506514-001C 6127/05 9 26 AM 7/02/05 7/02/05 12 44 PM 0506514-002C 6127/05 9 53 AM 7102/05 7102/05 t 26 PM <br />' 0506514-003C 6/27105 10 22 AM 7/02105 7102/05 11 28 AM 0506514-004C 6/27/05 10 37 AM 7102105 7102105 12 13 PM <br /> 0506514-005C 6/27/05 10 55 AM 7102/05 7102105 2 53 PM 0506514-006C 6127/05 11 13 AM 7102105 7102/05 4 03 PM <br /> 0506514-0070 6/27/05 It 37 AM 7/02105 7/02/05 4 53 PM 0506514-008C 6/27/05 12 24 PM 7102/05 7102105 5 41 PM <br />' 0506514-009C 6127/05 1119 PM 7/02105 7102105 6 30 PM 0506514-0 l OC 6127/05 12 55 PM 7/02105 7/02/05 7 17 PM <br /> 0506514-01 IC 6/27105 1 11 PM 7/02105 7/02105 8 03 PM 0506514-012C 6/27/05 1 30 PM 7/02105 7102/05 8 48 PM <br /> MS=Matnx Spike,MSD=Matrix Spike Duplicate LCS=Laboratory Control Sample LCSD=Laboratory Control Sample Duplicate RPD=Relative Percent Deviation <br /> %Recovery=1D"(MS-Sample)/(Amount Spiked),RPD=100.(MS- MSD)/((MS+MSD)12) <br /> MS I MSD spike recoveries and I or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons a)the sample is Inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked or b)the spiked sample's matrix Interferes with the spike recovery <br /> NIA=not enough sample to perform matrix spike and matrix spike duphcate <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matnx or analyte content <br /> borato extracLon solvents such as meth one chloride and acetone mayoccamonally a ar In the method blank at lowlevels <br /> IDHS Certification No 1644 W,,,.,QA/QC Officer <br />