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110 2nd Avenue South #D7 Pacheco,CA 94553-5560 <br /> McCampbell Analytical, Inc. Telcphone 925-798 1620 Fax 925 798-1622 <br />' 24 Website www mccarnphell com E mail niam@mccampbell cont <br /> Advanced GeoEnvironmcntal,Inc Client Protect 1D Three B's Date Sampled 06/28/05 <br />' 837 Shaw Road Date Received 06/29/05 <br /> Stockton, CA 95215 Client Contact Tun Cuellar Date Extracted 07/02/05 <br />' Client P O Date Analyzed 07/02/05 <br /> Oxygenated Volatile Organics+EDB and 1,2-DCA by P&T and GC/MS* <br />' Extraction Method SW5030B AnalytlLal Method.SW9260B Work Order 0506539 <br /> Lab 1D 0506539-009C 0506539-0140 0506539-OI 1C { 0506539-012C <br /> Client MW8E MW8F MW10A MW10B <br /> t _ ____— _ Reporting Limit for <br /> Matrix W W W j W DF-1 <br /> I <br /> DF I—-- I 1 1 S W <br /> ICompound Concentration ug/kg Agri- <br />' tent-Amyl methyl ethei (TAME) ND ND — ND ND NA 05 <br /> i <br /> t-Butyl alcohol(TBA) ND ND 35 ND NA 50 <br />' 1,2-Dtbromoethane(EDB) _ ND ND ND ND NA 05 <br /> 1,2-Dlchlorocthane(1,2-DCA) ND ND 93 071 NA 0 5 <br /> Dusopropyl ether(D1PF) ND _ ND ND ND NA 0 5 <br />' Ethyl tert-butyl ether(ETBE) ND ND ND ND NA 05 <br /> Methyl-t-butyl ether(MTBE) ND ND 66 19 NA 0 5 <br /> ISurrogate Recoveries(%) <br /> %SS 112 112 107 I o7 <br />' Comments <br /> "water and vapor samples are i eported toµg/L,soil/sludge/solid samples to mg/kg,production/non-aqueous liquid samples and all TCLP&SPLP <br />' extracts are reported to mg/L,wipe samples toµg/wipe <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> #surrogate diluted out o1 range or coelutes with another peak,&)low surrogate due to matrix interference <br />' h)lighter than water immtscible sheen/product iG present,i)liquid sample that contains greater than–1 vol %sediment,])sample diluted due to high <br /> organic contentlmatnx interference,k)reporting limit near,but not identical to our standard reporting limit due to variable Encore sample weight,m) <br /> reporting limit rarsed due to msuffictent sam le amount,n results are reported on a d!l wci ht basis, see attached narrative <br /> I <br /> I <br /> IDHS Certification No 1644 _ ___Angela Rydelius, Lab Manager <br />