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I110 2nd Avenue South,#137 Pacheco CA 94553-5560 <br /> McCampbell Analytical, Inc. Telephone 925-798-1620 Fax 925 798-1622 <br /> A#— I Website www mccampbell com E-mail main®mccarnpbell coin <br /> Advanced GeoEuvironmental,Inc Client Project ID Three B's Date Sampled 03/30/05 <br />' 837 Shaw Road Date Received 03/31/05 <br /> Client Contact Tun Cuellar Date Extracted 04/02/05-04/05/05 <br /> Stockton, CA 95215 <br /> Client P O Date Analyzed 04/02/05-04/05105 <br /> Oxygenated Volatile Organics+EDB and 1,2-DCA by P&T and GC/MS* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0503558 <br />' Lab ID 0503558-OO1C 0503558-002C 0503558-003C 0503558-004C <br /> Client 1D MW1 MW2 MW4 MW5 Reporting Limit for <br />' DF=1 <br /> Matrix W W W W <br /> DF 3 3 10 1 1 S W <br />' Compound Concentration ug/kg µg/L <br /> tert-Amyl methyl ether(TAME) ND<1 7 ND<5 0 ND ND NA 05 <br /> t-Butyl alcohol(TBA) 67 ND<50 13 ND NA 50 <br />' 1,2-Dibromoethane(EDB) ND<l 7 ND<5 0 ND ND NA 0 5 <br /> 1,2-Dichloroethane(1,2-DCA) ND<l 7 ND<5 0 ND ND NA 05 <br />' Ditsopropyl ether(DIPE) ND<l 7 ND<5 0 ND ND NA 0 5 <br />' Ethyl tert-butyl ether(ETRE) ND<l 7 ND<5 0 ND ND NA 0 5 <br /> Methyl-t-butyl ether(MTBE) 28 ND<5 0 23 1 3 NA 0 5 <br /> tSurrogate Recoveries(%) <br /> %SS 94 89 87 90 <br /> Comments J <br /> T- <br /> *water and vapor samples are reported in pg/L,soil/sludge/solid samples 1n mg/kg,pmduct/oil/non-aqueous liquid samples and all TCLP&SPLP <br />' extracts are reported to mg/L,wipe samples 1n lig/wipe <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysts <br /> #surrogate diluted out of range Or surrogate coelutes with another peak <br />' h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—1 vol %sediment,J)sample diluted due to high <br /> organic content/matnx interference,k)reporting limit near,but not identical to our standard reporting limit due to variable Encore sample weight,m) <br /> re2orting limit raised due to insufficient sample amount,n results are reported on a dry weight basis, see attached narrative <br /> • <br /> DHS Certification No 1644 Angela Rydelius, Lab Manager <br />