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110 2nd Avenue South 4D7 Pacheco CA 94553 5560 <br /> McCampbell Analytical, Inc. Telephone 925-798-1620 Fax 925-798-1622 <br />' Z4 1 Website www mccarMbell corn E mail main©mecampbeli com <br /> Advanced GeoEnvironmental,Inc Client Project ID Three B's Date Sampled 03/29/05 <br />' 837 Shaw Road Date Received 03/30/05 <br /> Client Contact Tun Cuellar Date Extracted 04/01/05-04/02/05 <br /> Stockton, CA 95215 Client P O Date Analyzed 04/01/05-04/02/05 <br /> I <br /> Oxygenated Volatile Organics+EDB and 1,2-DCA by P&T and GC/MS* <br />' <br /> ExtractionMethod SW5030B Analytical Method SW826013 Work Order 0503533 <br /> Lab ID 0503533-009C 0503533-0100 0503533-011C 0503533-012C <br /> f <br /> Client ID MW 10C MW 10D MW 10E MW 10F Reporting Limit for <br />' Matrix W W W W DF=1 <br /> DF l I 1 1 S W <br />' Compound Concentration Ug/kg 4g/L <br />' tert-Amyl methyl ether(TAME) ND ND ND ND NA 05 <br /> t-Butyl alcohol(TBA) ND ND ND ND NA 50 <br />' 1,2-Dibromoethane(EDB) ND ND ND ND NA 05 <br /> 1,2-Dichloroethane(1,2-DCA) ND ND ND ND NA 05 <br />' Dnsopropyl ether(DFPE) ND ND ND ND NA 0 5 <br />' Ethyl cert-butyl ether(ETBE) ND ND ND ND NA 05 <br /> Methyl-t-butyl ether(MTBE) 54 ND ND ND NA 0 5 <br />' Surrogate Recoveries{%) <br /> °/uS5 92 96 92 94 <br />' Comments <br /> *water and vapor samples are reported to pg/L,soil/sludge/solid samples in mg/kg,product/oil/non-aqueous liquid samples and all TCLP&SPLP <br />' extracts are reported in mg/L,wipe samples in ug/wipe <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysts <br />' #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—1 vol %sediment,l)sample diluted due to high <br /> organic content/matrix interference,k)reporting limit near,but not identical to our standard reporting limit due to variable Encore sample weight,m) <br /> reporting limit raised due to msuffietent sample amount,n results arc re orted on a dryweght basis,p,see attached narrative <br /> 1 <br /> 1 <br /> 1 <br /> DHS Certification No 1644 I.A_ —Angela Rydelius, Lab Manager <br /> 1 <br />