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i <br /> 110 2nd Avenue South,#D7 Pacheco,CA 94553 5560 <br /> McCampbell Analytical, Inc. Telephone 925 798-1620 Fax 925-798-1622 <br /> Z4 1 Website www mccampbell corn E-mail main@mccampbell com <br /> QC SUMMARY REPORT FOR SW8015C <br /> W O Sample Matrix Water QC Matrix Water WorkOrder 0503533 <br />' EPA Method SW6015C Extraction SW3510C BatchlD 15645 Spiked Sample ID "/A <br /> Analyte Sample Spiked MS' MSD' MS-MSD` LCS LCSD LCS-LCSD Acceptance Criteria (%) <br /> pg/L pg/L %Rec % Rec %RPD %Rec % Rec %RPD MS I MSD LCS 1 LCSD <br />' TPH(d) NIA 1000 NIA N/A N/A 117 117 0 NIA 70- 130 <br /> %SS N/A 2500 N/A NIA N/A 96 97 141 N/A 70- 130 <br />' All target compounds to the Method Blank of this extraction batch were ND less than the method RL with the following exceptions <br /> NONE <br /> I <br /> BATCH 15845 SUMMARY <br />' Sample ID Date Sampled Date Extracted Date Analyzed Sample ID Date Sampled Date Extracted Date Analyzed <br /> 0503533-OOIB 3/29/05 10 45 AM 3/30/05 9 03 AM 3131/05 4 07 AM 0503533-002B 3/29105 8 59 AM 3130105 9 03 AM 3131/05 5 15 AM <br /> 0503533-003B 3129105 9 18 AM 3130/05 9 03 AM 3/31/05 6 23 AM 0503533-004B 3129105 9 38 AM 3/30105 9 03 AM 4/01105 10 32 PM <br /> 0503533-005B 3129105 10 01 AM 3130105 9 03 AM 3/31/05 3 27 AM 0503533-0068 3/29/05 10 24 AM 3130/05 9 03 AM 3131105 4 33 AM <br />' 0503533-007B 3129105 11 30 AM 3130105 9 03 AM 3/31/05 5 38 AM 0503533-008B 3/29/05 12 01 PM 3130105 9 03 AM 3/31/05 12 28 PM <br /> 0503533-009B 3129105 12 23 PM 3130105 9 03 AM 3/31105 1 38 PM 0503533-OIOB 3129105 12 47 PM 3/30105 9 03 AM 3/31/05 3 47 PM <br /> I <br /> 1 <br /> I <br /> MS=Metrix Spike MSD=Matrix Spike Duplicate LCS=Laboratory Control Sample LCSD=Laboratory Control Sample Duplicate RPD=Relative Percent Deviation <br />' %Recovery=100'(MS-Sample)/(Amount Spiked),RPD=100'(MS- MSD)1((MS+MSD)1 2) <br /> 'MS/MSD spike recoveries and I or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons a)the sample is inhomogenous <br /> AND contains significant concentrations of analyte relative to the amount spiked or b)the spiked sample s matrix interferes wth the spike recovery <br />' <br /> NIA=not enough sample to perform matrix spike and matrix spike duplicate <br /> NR=analyte concentration in sample exceeds spike amount for soil malnx or exceeds 2x spike amount for water matrix or sample diluted due to hooh matrix or analyte content <br /> WS Certification No 1644 QA/QC Officer <br /> I <br />