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1 <br /> McCampbell Analytical, Inc. 110 2nphoneAvenSouth -16 Pacheco CA 98 1622560 <br />' Telephone 925-798-1620 Fax 925-798 1622 <br /> Z4 Website www mccampbell corn E mail main@mccampbelt com <br /> Advanced GeoEnvironmental,Inc Client Project ID Three B's Date Sampled 12/28/04 <br />' 837 Shaw Road Date Received 12/29/04 <br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 12/30/04-01/05/05 <br />' Client P O Date Analyzed 12/30/04-01105/05 <br /> Oxygenated Volatile Organics+EDB and 1,2-DCA by P&T and GC/MS* <br />' Extraction Method SW5030B Analytical Method SW8260B Work Order 0412541 <br /> Lab ID 0412541-009C 0412541-OIOC 0412541-011C 0412541-012C <br /> Client ID MW8C MW8D MW8E MW8F Reporting Limit for <br /> tMatrix W W W W DF=1 <br /> DF 1 1 1 1 S W <br /> Compound Concentration ug/kg lig/L <br />' tert-Amyl methyl ether(TAME) ND ND ND ND NA 05 <br /> t-Butyl alcohol(TBA) ND ND ND ND NA 50 <br /> 1,2-Dibromoethane(EDB) ND ND ND ND NA 0 5 <br /> 1,2-Dichloroethane(1,2-DCA) ND ND ND ND NA 0 5 <br /> lie Dnsopropyl ether(DIPE) ND ND ND ND NA 0 5 <br /> Ethyl tert-butyl ether(ETBE) ND ND ND ND NA 05 <br /> Methyl-t-butyl ether(MTBE) 050 ND ND ND NA 05 <br /> Surrogate Recoveries(%) <br /> %SS 102 101 102 102 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in pg/L,soil/sludge/solid samples in pg/kg, wipe samples in pg/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—1 vol %sediment,j)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Angela Rydehus, Lab Manager <br />