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' 110 2nd Avenue South #D7 Pacheco CA 94553 5560 <br /> McCampbell Analytical, Inc. Telephone 925-798 1620 Fax 925-798 1622 <br /> Zo Website www mccampbell corn E-mail unm@mccanipbell com <br /> IAdvanced GeoEnvironmental, Inc Client Project ID Three B's Date Sampled 09/15/04 <br />' 837 Shaw Road <br /> Date Received 09/16/04 <br /> Client Contact Tim Cuellar Date Extracted 09/18/04 <br /> Stockton, CA 95215 <br />' Client P O Date Analyzed 09/18/04 <br /> . --i I <br /> Oxygenated Volatile Organics+EDB and 1,2-DCA by P&T and GC/VIS* <br /> Fxtraction Method SW5030B Analytic-1 Method SW8260B Work Order 0409235 <br /> ILab 1D 0409235-OOIC 0409235-002C 0409235-003C 0409235-004C <br /> Client ID MWSA/9/15/04 MW813/9/15/04 MW8C/9/15/04JMW8D/9115104 <br /> Reporting Limit for <br />' Matrix W W W W — DC=1 <br /> DF 10 1 1 1 S W <br /> Compound Concentration ug/kg µg/L <br /> I <br /> i <br /> tent-Amyl methyl ether(TAME) ND<5 0 ND ND ND NA 05 <br /> t-Butyl alcohol(TBA) ND<50ND ND ND NA 5 0 <br /> 1,2-DEbromoethane(EDB) ND<5 0 I NDND ND NA 05 <br /> 1,2-Dichloroethane(1,2-DCA) ND<5 0 ND ND NU NA 05 <br /> k <br /> Dnsoprapyl ether(DIPS) ND<5 0 ND ND ND NA 05 <br /> Ethyl Cert-butyl ether(ETBE) ND<5 0 ND ND ND NA 0 5 <br /> Methyl-t-butvl ether(MTBE) 110 089 ND ND NA 05 <br /> Surrogate Recoveries (%) <br /> i <br /> %SS 93 8 980 95 7 904 <br /> Comments <br /> E <br /> *water and vapor samples and all TCLP&SPLP extracts are reported toµg/L,soiUsludgelsolid samples inµg/kg, wipe samples in jig/wipe <br /> product/oil/non-aqueous liquid samples in mg/L. <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysts <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br />' h)lighter than water immiscible sheen/product is present i)liquid sample that contains greater than---1 vol %sediment j)sample diluted due to high <br /> organ ic content <br /> I <br /> DHS Certification No 1644 Angela Rydebus, Lab Manager <br />